tetrahydro-2-<<4-<4-(ethoxycarbonyl)pyridin-3-yl>phenyl>methoxy>-2H-pyran

Base Information

Chemical Name:tetrahydro-2-<<4-<4-(ethoxycarbonyl)pyridin-3-yl>phenyl>methoxy>-2H-pyran
CAS No.:164460-54-2
Molecular Formula:C₂₀H₂₃NO₄
Molecular Weight:341.407
Hs Code.:

Synonyms:tetrahydro-2-<<4-<4-(ethoxycarbonyl)pyridin-3-yl>phenyl>methoxy>-2H-pyran

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Chemical Property of tetrahydro-2-<<4-<4-(ethoxycarbonyl)pyridin-3-yl>phenyl>methoxy>-2H-pyran

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Technology Process of tetrahydro-2-<<4-<4-(ethoxycarbonyl)pyridin-3-yl>phenyl>methoxy>-2H-pyran

There total 1 articles about tetrahydro-2-<<4-<4-(ethoxycarbonyl)pyridin-3-yl>phenyl>methoxy>-2H-pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13959-01-8
ethyl 3-bromopyridine-4-carboxylate

: 164460-51-9
<4-<<(tetrahydro-2H-pyran-2-yl)oxy>methyl>phenyl>boronic acid

: 164460-54-2
tetrahydro-2-<<4-<4-(ethoxycarbonyl)pyridin-3-yl>phenyl>methoxy>-2H-pyran

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; Yield given. Multistep reaction; 1.) 1,2-DME, RT, 30 min, 2.) 1,2-DME, reflux;
DOI:10.1021/jm00049a012

Reference yield: 97.0%

: 164460-54-2
tetrahydro-2-<<4-<4-(ethoxycarbonyl)pyridin-3-yl>phenyl>methoxy>-2H-pyran

: 164460-33-7
ethyl 3-<4-(hydroxymethyl)phenyl>pyridine-4-carboxylate

Guidance literature:: With toluene-4-sulfonic acid; In methanol; Heating;
DOI:10.1021/jm00049a012

Reference yield:

: 164460-54-2
tetrahydro-2-<<4-<4-(ethoxycarbonyl)pyridin-3-yl>phenyl>methoxy>-2H-pyran

: 164460-37-1
3-(4-Chloromethyl-phenyl)-isonicotinic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / p-TsOH*H₂O / methanol / Heating

2: 1.) 1N HCl, 2.) thionyl chloride / 1.) EtOH, 2.) CHCl₃, RT

With hydrogenchloride; thionyl chloride; toluene-4-sulfonic acid; In methanol;
DOI:10.1021/jm00049a012