(S)-methyl-6-methyl-4-(3-nitrophenyl)-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate

Base Information

Chemical Name:(S)-methyl-6-methyl-4-(3-nitrophenyl)-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate
CAS No.:108932-26-9
Molecular Formula:C₁₃H₁₃N₃O₄S
Molecular Weight:307.33
Hs Code.:

Synonyms:(S)-methyl-6-methyl-4-(3-nitrophenyl)-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-methyl-6-methyl-4-(3-nitrophenyl)-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate

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Technology Process of (S)-methyl-6-methyl-4-(3-nitrophenyl)-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate

There total 3 articles about (S)-methyl-6-methyl-4-(3-nitrophenyl)-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 99-61-6
3-nitro-benzaldehyde

: 105-45-3
acetoacetic acid methyl ester

: 17356-08-0
thiourea

: 134074-33-2,108932-24-7,108932-26-9
methyl 4-(3-nitrophenyl)-6-methyl-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate

Guidance literature:: With iodine; at 60 ℃; for 0.333333h; Microwave irradiation;
DOI:10.1080/00397911.2011.593289

Reference yield: 94.0%

: 99-61-6
3-nitro-benzaldehyde

: 105-45-3
acetoacetic acid methyl ester

: 17356-08-0
thiourea

: 108932-26-9
(S)-methyl-6-methyl-4-(3-nitrophenyl)-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate

Guidance literature:: 3-nitro-benzaldehyde; thiourea; With (S)-6,6'-di(naphthalen-1-yl)-1,1'-spirobiindane-7,7'-diyl phosphate; In 5,5-dimethyl-1,3-cyclohexadiene; at 20 ℃; for 2h; Inert atmosphere;

acetoacetic acid methyl ester; In 5,5-dimethyl-1,3-cyclohexadiene; at 50 ℃; for 72h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1039/c2ob25663k