perdeutero-o-benzyne

Base Information

• Chemical Name: perdeutero-o-benzyne
• CAS No.: 67356-66-5
• Molecular Formula: C₆H₄
• Molecular Weight: 80.066
• Mol file: 67356-66-5.mol

Synonyms:perdeutero-o-benzyne

Chemical Property of perdeutero-o-benzyne

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of perdeutero-o-benzyne

There total 5 articles about perdeutero-o-benzyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

phthalic anhydride-d4 (75935-32-9) → perdeutero-o-benzyne (67356-66-5)

Guidance literature:

Irradiation;

DOI:10.1021/ja00027a007

Reference yield:

benzene-d6 (1076-43-3) → acetylene-d2 (1070-74-2) + phenyl-d5 (34346-16-2) + perdeutero-o-benzyne (67356-66-5) + triacetylene-d2 + 1,3-hexadien-5-yne-d6 + fulvene-d6

Guidance literature:

Product distribution; Mechanism; corona discharge; also with benzene;

DOI:10.1021/j100202a018

Reference yield:

phthalic anhydride-d4 (75935-32-9) → perdeutero-o-benzyne (67356-66-5) + [((2)H4)cyclopenta-2,4-dienylidene]ketene

Guidance literature:

Irradiation;

DOI:10.1021/ja00027a007

upstream raw materials:

phthalic anhydride-d₄

benzene-d6

C₆⁽²⁾H₅⁽¹⁺⁾

Refernces

• 1、 Radziszewski, Juliusz G.,Hess Jr., B. Andes,Zahradnik, Rudolf. "Infrared spectrum of o-benzyne: Experiment and theory". . p. 52 - 57. Retrieved 2007/10/02.