C₃₂H₃₉NO₆

Base Information

• Chemical Name: C₃₂H₃₉NO₆
• CAS No.: 1276112-33-4
• Molecular Formula: C₃₂H₃₉NO₆
• Molecular Weight: 533.665
• Mol file: 1276112-33-4.mol

Synonyms:C₃₂H₃₉NO₆

Chemical Property of C₃₂H₃₉NO₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₂H₃₉NO₆

There total 32 articles about C₃₂H₃₉NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

C32H38N2O5 (1422740-24-6) → C32H39NO6 (1276112-33-4)

Guidance literature:

With diisobutylaluminium hydride; In hexane; toluene; at -78 ℃; for 1h;

DOI:10.3762/bjoc.8.210

Reference yield:

C33H43NO7 (1308271-90-0) → C32H39NO6 (1276112-33-4)

Guidance literature:

With sodium periodate; In tetrahydrofuran; water; at 0 - 20 ℃; for 3.5h;

DOI:10.1016/j.tetlet.2011.01.018

Reference yield:

C27H27NO5 (1308271-84-2) → C32H39NO6 (1276112-33-4)

Guidance literature:

Multi-step reaction with 10 steps

1: sodium tetrahydroborate / methanol / 24 h / 0 - 20 °C

2: silver(l) oxide / N,N-dimethyl-formamide / 24 h / 20 °C

3: ammonium cerium (IV) nitrate / water; acetonitrile / 2.5 h / 0 - 20 °C

4: dmap; triethylamine / dichloromethane / 2 h / 0 °C

5: tetrahydrofuran / 1.5 h / -78 °C

6: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 2 h / 0 °C

7: pyridine / 12 h / 0 - 20 °C

8: tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium formate; triethylamine / toluene / 0.5 h / Reflux

9: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone; tert-butyl alcohol / 24 h / 20 °C

10: sodium periodate / tetrahydrofuran; water / 3.5 h / 0 - 20 °C

With pyridine; dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium cerium (IV) nitrate; cerium(III) chloride heptahydrate; ammonium formate; 4-methylmorpholine N-oxide; triethylamine; silver(l) oxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; tert-butyl alcohol;

DOI:10.1016/j.tetlet.2011.01.018

upstream raw materials:

C₂₇H₂₇NO₅

C₂₇H₂₉NO₅

C₃₄H₃₅NO₅

C₂₆H₂₇NO₄

Downstream raw materials:

C₃₀H₃₅NO₃

C₃₅H₄₅NO₇

C₃₄H₄₁NO₆

C₄₃H₆₁NO₆