benzyl 2-acetamido-2,4-dideoxy-6-O-mesyl-3-O--α-D-xylo-hexopyranoside

Base Information

Chemical Name:benzyl 2-acetamido-2,4-dideoxy-6-O-mesyl-3-O--α-D-xylo-hexopyranoside
CAS No.:78569-10-5
Molecular Formula:C₂₀H₂₉NO₉S
Molecular Weight:459.518
Hs Code.:

benzyl 2-acetamido-2,4-dideoxy-6-O-mesyl-3-O-<D-1-(methoxycarbonyl)ethyl>-α-D-xylo-hexopyranoside

Synonyms:benzyl 2-acetamido-2,4-dideoxy-6-O-mesyl-3-O--α-D-xylo-hexopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 2-acetamido-2,4-dideoxy-6-O-mesyl-3-O--α-D-xylo-hexopyranoside

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Technology Process of benzyl 2-acetamido-2,4-dideoxy-6-O-mesyl-3-O--α-D-xylo-hexopyranoside

There total 4 articles about benzyl 2-acetamido-2,4-dideoxy-6-O-mesyl-3-O--α-D-xylo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 124-63-0
methanesulfonyl chloride

: 78569-09-2
benzyl 2-acetamido-2,4-dideoxy-3-O--α-D-xylo-hexopyranoside

: 78569-10-5
benzyl 2-acetamido-2,4-dideoxy-6-O-mesyl-3-O--α-D-xylo-hexopyranoside

Guidance literature:: In pyridine; at 0 ℃;
DOI:10.1016/S0008-6215(00)85983-2

Reference yield:

: 78569-08-1
benzyl 2-acetamido-6-O-benzoyl-2,4-dideoxy-3-O--α-D-xylo-hexopyranoside

: 78569-10-5
benzyl 2-acetamido-2,4-dideoxy-6-O-mesyl-3-O--α-D-xylo-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / 1 M NaOMe / methanol / 0.5 h / Ambient temperature

2: 83 percent / pyridine / 0 °C

With sodium methylate; In pyridine; methanol;
DOI:10.1016/S0008-6215(00)85983-2

Reference yield:

: 78569-06-9
benzyl 2-acetamido-6-O-benzoyl-4-chloro-2,4-dideoxy-3-O--α-D-galactopyranoside

: 78569-10-5
benzyl 2-acetamido-2,4-dideoxy-6-O-mesyl-3-O--α-D-xylo-hexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / α,α'-azobis(isobutanonitrile), tributyltin hydride / toluene / 3 h / Heating

2: 97 percent / 1 M NaOMe / methanol / 0.5 h / Ambient temperature

3: 83 percent / pyridine / 0 °C

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium methylate; In pyridine; methanol; toluene;
DOI:10.1016/S0008-6215(00)85983-2