S-2-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-3,3-dimethyl-pent-4-enoic acid

Base Information

Chemical Name:S-2-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-3,3-dimethyl-pent-4-enoic acid
CAS No.:505067-02-7
Molecular Formula:C₂₆H₃₆O₃Si
Molecular Weight:424.656
Hs Code.:

Synonyms:S-2-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-3,3-dimethyl-pent-4-enoic acid

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Chemical Property of S-2-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-3,3-dimethyl-pent-4-enoic acid

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Technology Process of S-2-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-3,3-dimethyl-pent-4-enoic acid

There total 1 articles about S-2-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-3,3-dimethyl-pent-4-enoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 505067-47-0
5-(tert-butyl-diphenyl-silanyloxy)-pentanoic acid 3-methyl-but-2-enyl ester

: 505067-02-7
S-2-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-3,3-dimethyl-pent-4-enoic acid

: 2-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-3,3-dimethyl-pent-4-enoic acid

Guidance literature:: With BrB{[(CF₃)2C₆H₃SO₂]2NCHPh}2; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 - 20 ℃; Title compound not separated from byproducts;
DOI:10.1021/ol0275116

Reference yield: 52.0%

: 505067-02-7
S-2-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-3,3-dimethyl-pent-4-enoic acid

: S-3-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-4,4-dimethyl-5-methylene-dihydro-furan-2-one

Guidance literature:: With oxygen; copper dichloride; palladium dichloride; In water; N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1021/ol0275116