5-(tert-butyl-diphenyl-silanyloxy)-pentanoic acid 3-methyl-but-2-enyl ester

Base Information

Chemical Name:5-(tert-butyl-diphenyl-silanyloxy)-pentanoic acid 3-methyl-but-2-enyl ester
CAS No.:505067-47-0
Molecular Formula:C₂₆H₃₆O₃Si
Molecular Weight:424.656
Hs Code.:

Synonyms:5-(tert-butyl-diphenyl-silanyloxy)-pentanoic acid 3-methyl-but-2-enyl ester

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Chemical Property of 5-(tert-butyl-diphenyl-silanyloxy)-pentanoic acid 3-methyl-but-2-enyl ester

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Technology Process of 5-(tert-butyl-diphenyl-silanyloxy)-pentanoic acid 3-methyl-but-2-enyl ester

There total 2 articles about 5-(tert-butyl-diphenyl-silanyloxy)-pentanoic acid 3-methyl-but-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 118715-27-8
5-(tert-butyl-diphenyl-silanyloxy)-pentanoic acid

: 556-82-1
3-methyl-2-buten-1-ol

: 505067-47-0
5-(tert-butyl-diphenyl-silanyloxy)-pentanoic acid 3-methyl-but-2-enyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃;
DOI:10.1021/ol0275116

Reference yield:

: 179690-97-2
5-(tert-butyl-diphenyl-silanyloxy)-pentanoic acid methyl ester

: 505067-47-0
5-(tert-butyl-diphenyl-silanyloxy)-pentanoic acid 3-methyl-but-2-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / KOH / methanol; H₂O / 6 h / 20 °C

2: 76 percent / DCC; DMAP / CH₂Cl₂ / 20 °C

With dmap; potassium hydroxide; dicyclohexyl-carbodiimide; In methanol; dichloromethane; water;
DOI:10.1021/ol0275116

Reference yield: 80.0%

: 505067-47-0
5-(tert-butyl-diphenyl-silanyloxy)-pentanoic acid 3-methyl-but-2-enyl ester

: d,l-2-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-3,3-dimethyl-pent-4-enoic acid

Guidance literature:: With tert-butyldimethylsilyl chloride; lithium hexamethyldisilazane; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 - 20 ℃;
DOI:10.1021/ol0275116