2'-Methyl-3,4',5,6'-tetramethoxy-diphenylaether

Base Information

Chemical Name:2'-Methyl-3,4',5,6'-tetramethoxy-diphenylaether
CAS No.:93728-36-0
Molecular Formula:C₁₇H₂₀O₅
Molecular Weight:304.343
Hs Code.:

Synonyms:2'-Methyl-3,4',5,6'-tetramethoxy-diphenylaether

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2'-Methyl-3,4',5,6'-tetramethoxy-diphenylaether

Chemical Property:

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Technology Process of 2'-Methyl-3,4',5,6'-tetramethoxy-diphenylaether

There total 4 articles about 2'-Methyl-3,4',5,6'-tetramethoxy-diphenylaether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 93653-84-0
2-Chlor-2'-methyl-3,4',5,6'-tetramethoxy-diphenylaether

: 93728-36-0
2'-Methyl-3,4',5,6'-tetramethoxy-diphenylaether

Guidance literature:: With potassium hydroxide; hydrogen; palladium on activated charcoal; In methanol; at 50 ℃; under 38000 Torr;
DOI:10.1002/hlca.19620450311

Reference yield:

: 94572-36-8
2-Chlor-4'-hydroxy-2'-methyl-3,5,6'-trimethoxy-diphenylaether

: 93728-36-0
2'-Methyl-3,4',5,6'-tetramethoxy-diphenylaether

Guidance literature:: Multi-step reaction with 2 steps

1: methanol

2: H₂, KOH / Pd-C / methanol / 50 °C / 38000 Torr

With potassium hydroxide; hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1002/hlca.19620450311

Reference yield:

: 25357-24-8
2-chloro-4′-hydroxy-6-methoxycarbonyl-2′-methyl-3,5,6′-trimethoxydiphenyl ether

: 93728-36-0
2'-Methyl-3,4',5,6'-tetramethoxy-diphenylaether

Guidance literature:: Multi-step reaction with 4 steps

1: aq. NaOH

2: H₂SO₄ / acetic acid

3: methanol

4: H₂, KOH / Pd-C / methanol / 50 °C / 38000 Torr

With potassium hydroxide; sodium hydroxide; sulfuric acid; hydrogen; palladium on activated charcoal; In methanol; acetic acid;
DOI:10.1002/hlca.19620450311