N-<(phenyloxy)carbonyl>-6-ethynyl-10-oxo-3-(trimethylacetoxy)-5,6,7,8,9,10-hexahydrophenanthridine

Base Information

Chemical Name:N-<(phenyloxy)carbonyl>-6-ethynyl-10-oxo-3-(trimethylacetoxy)-5,6,7,8,9,10-hexahydrophenanthridine
CAS No.:144019-83-0
Molecular Formula:C₂₇H₂₅NO₅
Molecular Weight:443.499
Hs Code.:

Synonyms:N-<(phenyloxy)carbonyl>-6-ethynyl-10-oxo-3-(trimethylacetoxy)-5,6,7,8,9,10-hexahydrophenanthridine

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Chemical Property of N-<(phenyloxy)carbonyl>-6-ethynyl-10-oxo-3-(trimethylacetoxy)-5,6,7,8,9,10-hexahydrophenanthridine

Chemical Property:

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Technology Process of N-<(phenyloxy)carbonyl>-6-ethynyl-10-oxo-3-(trimethylacetoxy)-5,6,7,8,9,10-hexahydrophenanthridine

There total 3 articles about N-<(phenyloxy)carbonyl>-6-ethynyl-10-oxo-3-(trimethylacetoxy)-5,6,7,8,9,10-hexahydrophenanthridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 144019-82-9,144071-06-7
N-[(Phenyloxy)carbonyl]-10-[(tert-butyldimethylsilyl)oxy)-6a,10a-epoxy-6-ethynyl-3-(trimethylacetoxy)-5,6,6a,7,8,9,10,10a-octahydrophenanthridine

: 60-29-7,927820-24-4
diethyl ether

: 144019-83-0
N-<(phenyloxy)carbonyl>-6-ethynyl-10-oxo-3-(trimethylacetoxy)-5,6,7,8,9,10-hexahydrophenanthridine

Guidance literature:: With BF_3.OEt₂; In chloroform; benzene;

Reference yield:

: 144019-82-9,144071-06-7
N-<(phenyloxy)carbonyl>-10-<(tert-butyldimethylsilyl)oxy>-6a,10a-epoxy-6-ethynyl-3-(trimethylacetoxy)-5,6,6a,7,8,9,10,10a-octahydrophenanthridine

: 144019-83-0
N-<(phenyloxy)carbonyl>-6-ethynyl-10-oxo-3-(trimethylacetoxy)-5,6,7,8,9,10-hexahydrophenanthridine

Guidance literature:: With boron trifluoride diethyl etherate; water; silica gel; Yield given. Multistep reaction; 1.) CHCl₃, 25 deg C, 1.5 h, 2.) CHCl₃, 25 deg C, 12 h;
DOI:10.1021/ja00049a023