Bis--arsinchlorid

Base Information

• Chemical Name: Bis--arsinchlorid
• CAS No.: 13904-19-3
• Molecular Formula: C₁₂AsClF₁₀
• Molecular Weight: 444.491
• Mol file: 13904-19-3.mol

Synonyms:Bis--arsinchlorid

Chemical Property of Bis--arsinchlorid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Bis--arsinchlorid

There total 3 articles about Bis--arsinchlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

Bis{bis(pentafluorphenyl)arsanyl}sulfan (18207-53-9) → Bis--arsinchlorid (13904-19-3)

Guidance literature:

With mercury dichloride; In diethyl ether; byproducts: HgS;

DOI:10.1039/j19680000483

Reference yield: 77.0%

dichloro-dimethylamino-arsine (31012-32-5) + 2,3,4,5,6-pentafluorophenylmagnesium bromide (879-05-0) → Bis--arsinchlorid (13904-19-3)

Guidance literature:

In diethyl ether; in boiling ether; filtration, evapn., extn.(pentane), distn.;

DOI:10.1039/j19680000483

Reference yield:

→ Bis--arsinchlorid (13904-19-3)

Guidance literature:

C6F5-MgBr, dimethylaminoarsenous dichloride;

DOI:10.1039/j19680000483

upstream raw materials:

dichloro-dimethylamino-arsine

2,3,4,5,6-pentafluorophenylmagnesium bromide

Bis{bis(pentafluorphenyl)arsanyl}sulfan

Downstream raw materials:

tetrakis(pentafluorophenyl)diarsenic(III) oxide

tetrakis(pentafluorophenyl)diarsine

tris(pentafluorophenyl)arsine oxide

Pentafluorobenzene