Carbamic acid, (4-amino-2-butenyl)-, 1,1-dimethylethyl ester, (Z)- (9CI)

Base Information

• Chemical Name: Carbamic acid, (4-amino-2-butenyl)-, 1,1-dimethylethyl ester, (Z)- (9CI)
• CAS No.: 167845-56-9
• Molecular Formula: C₉H₁₈N₂O₂
• Molecular Weight: 186.254
• Mol file: 167845-56-9.mol

Synonyms:Carbamic acid, (4-amino-2-butenyl)-, 1,1-dimethylethyl ester, (Z)- (9CI)

Chemical Property of Carbamic acid, (4-amino-2-butenyl)-, 1,1-dimethylethyl ester, (Z)- (9CI)

Chemical Property:

• PSA: 64.35000
• LogP: 2.11720

Purity/Quality:

1-N-Boc-2-cis-butene-1,4-diamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Carbamic acid, (4-amino-2-butenyl)-, 1,1-dimethylethyl ester, (Z)- (9CI)

There total 2 articles about Carbamic acid, (4-amino-2-butenyl)-, 1,1-dimethylethyl ester, (Z)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.7%

di-tert-butyl dicarbonate (24424-99-5) + cis-1,4-diamino-2-butene (40794-72-7) → (Z)-(4-aminobut-2-en-1-yl) tert-butyl carbamate (167845-56-9,1807939-98-5) + (4-(tert-butoxycarbonylamino)but-2-enyl)carbamic acid tert-butyl ester (215167-64-9)

Guidance literature:

In ethanol; at 20 ℃;

Reference yield:

N2 H4 + 1-N-(t-Butoxycarbonyl)amino-4-phthalimido-2,Z-butene (167845-55-8) → (Z)-(4-aminobut-2-en-1-yl) tert-butyl carbamate (167845-56-9,1807939-98-5)

Guidance literature:

In methanol; water;

upstream raw materials:

1-N-(t-Butoxycarbonyl)amino-4-phthalimido-2,Z-butene

di-tert-butyl dicarbonate

cis-1,4-diamino-2-butene