Technology Process of C16H26NO5P
There total 5 articles about C16H26NO5P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Dimethyl phosphite;
With
sodium hydride;
In
tetrahydrofuran;
at 0 ℃;
for 0.166667h;
tert-butyl (R)-4-benzyl-1,2,3-oxathiazolidine-3-carboxylate-2,2-dioxide;
In
tetrahydrofuran;
at 65 ℃;
for 11.5h;
DOI:10.1016/j.tetlet.2011.04.115
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium periodate; ruthenium(III) chloride trihydrate / acetonitrile / 6 h / 0 °C
2.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C
2.2: 11.5 h / 65 °C
With
sodium periodate; ruthenium(III) chloride trihydrate; sodium hydride;
In
tetrahydrofuran; acetonitrile;
DOI:10.1016/j.tetlet.2011.04.115
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine / dichloromethane / 2 h / 20 °C
2.1: 1H-imidazole; thionyl chloride; triethylamine / dichloromethane / 2 h / 0 - 20 °C
3.1: sodium periodate; ruthenium(III) chloride trihydrate / acetonitrile / 6 h / 0 °C
4.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C
4.2: 11.5 h / 65 °C
With
1H-imidazole; sodium periodate; thionyl chloride; ruthenium(III) chloride trihydrate; sodium hydride; triethylamine;
In
tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1016/j.tetlet.2011.04.115
