3-(benzyloxycarbonylamino)propyl-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Base Information

Chemical Name:3-(benzyloxycarbonylamino)propyl-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranoside
CAS No.:932015-08-2
Molecular Formula:C₃₉H₃₆N₂O₁₁
Molecular Weight:708.722
Hs Code.:

Synonyms:3-(benzyloxycarbonylamino)propyl-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

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Chemical Property of 3-(benzyloxycarbonylamino)propyl-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

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Technology Process of 3-(benzyloxycarbonylamino)propyl-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

There total 15 articles about 3-(benzyloxycarbonylamino)propyl-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: C₄₁H₃₈N₂O₁₂

: 932015-08-2
3-(benzyloxycarbonylamino)propyl-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With acetyl chloride; In methanol; dichloromethane; at 0 - 20 ℃; for 16h;

Reference yield:

: 99409-32-2
ethyl-3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 932015-08-2
3-(benzyloxycarbonylamino)propyl-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium methylate / methanol / 2.5 h / 20 °C

2.1: pyridine / 4 h / 50 °C

2.2: 3.33 h / 10 - 20 °C

3.1: water; acetic acid / 2 h / 70 °C

4.1: pyridine / toluene / 18 h / 25 °C

5.1: N-iodo-succinimide / dichloromethane / 0.5 h / 20 °C / Molecular sieve

5.2: 22 - 27 °C

6.1: acetyl chloride / dichloromethane; methanol / 16 h / 0 - 20 °C

With pyridine; N-iodo-succinimide; water; sodium methylate; acetic acid; acetyl chloride; In methanol; dichloromethane; toluene;

Reference yield:

: 130539-43-4
ethyl 2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 932015-08-2
3-(benzyloxycarbonylamino)propyl-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine / 4 h / 50 °C

1.2: 3.33 h / 10 - 20 °C

2.1: water; acetic acid / 2 h / 70 °C

3.1: pyridine / toluene / 18 h / 25 °C

4.1: N-iodo-succinimide / dichloromethane / 0.5 h / 20 °C / Molecular sieve

4.2: 22 - 27 °C

5.1: acetyl chloride / dichloromethane; methanol / 16 h / 0 - 20 °C

With pyridine; N-iodo-succinimide; water; acetic acid; acetyl chloride; In methanol; dichloromethane; toluene;