3-(4-chlorobenzoyl)-2-ethoxycarbonyl-2,3-dihydro-2-methyl-5-methylthio-1,3,4-thiadiazole

Base Information

• Chemical Name: 3-(4-chlorobenzoyl)-2-ethoxycarbonyl-2,3-dihydro-2-methyl-5-methylthio-1,3,4-thiadiazole
• CAS No.: 138612-39-2
• Molecular Formula: C₁₄H₁₅ClN₂O₃S₂
• Molecular Weight: 358.87

Synonyms:3-(4-chlorobenzoyl)-2-ethoxycarbonyl-2,3-dihydro-2-methyl-5-methylthio-1,3,4-thiadiazole

Chemical Property of 3-(4-chlorobenzoyl)-2-ethoxycarbonyl-2,3-dihydro-2-methyl-5-methylthio-1,3,4-thiadiazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(4-chlorobenzoyl)-2-ethoxycarbonyl-2,3-dihydro-2-methyl-5-methylthio-1,3,4-thiadiazole

There total 1 articles about 3-(4-chlorobenzoyl)-2-ethoxycarbonyl-2,3-dihydro-2-methyl-5-methylthio-1,3,4-thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

4-chloro-benzoyl chloride (122-01-0) + ethyl 2-(2-((methylthio)carbonothioyl)hydrazono)propanoate (93771-60-9) → 3-(4-chlorobenzoyl)-2-ethoxycarbonyl-2,3-dihydro-2-methyl-5-methylthio-1,3,4-thiadiazole (138612-39-2)

Guidance literature:

In chloroform; for 4h; Heating;

DOI:10.3987/COM-91-5813

Reference yield: 86.0%

3-(4-chlorobenzoyl)-2-ethoxycarbonyl-2,3-dihydro-2-methyl-5-methylthio-1,3,4-thiadiazole (138612-39-2) → 3-(4-chlorobenzoyl)-2-ethoxycarbonyl-2,3-dihydro-2-methyl-5-methylsulfinyl-1,3,4-thiadiazole (138612-41-6,138612-51-8)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; for 1h; Ambient temperature;

DOI:10.3987/COM-91-5813

Reference yield: 86.0%

3-(4-chlorobenzoyl)-2-ethoxycarbonyl-2,3-dihydro-2-methyl-5-methylthio-1,3,4-thiadiazole (138612-39-2) → 3-(4-chlorobenzoyl)-2,3-dihydro-2-hydroxycarbonyl-2-methyl-5-methylthio-1,3,4-thiadiazole (138612-40-5)

Guidance literature:

With potassium hydroxide; In methanol; for 6h; Ambient temperature;

DOI:10.3987/COM-91-5813

upstream raw materials:

4-chloro-benzoyl chloride

ethyl 2-(2-((methylthio)carbonothioyl)hydrazono)propanoate

Downstream raw materials:

3-(4-chlorobenzoyl)-2,3-dihydro-2-hydroxycarbonyl-2-methyl-5-methylthio-1,3,4-thiadiazole

3-(4-chlorobenzoyl)-2-ethoxycarbonyl-2,3-dihydro-2-methyl-5-methylsulfinyl-1,3,4-thiadiazole

3-(4-chlorobenzoyl)-2,3-dihydro-3-hydroxycarbonyl-2-methyl-5-phenylthio-1,3,4-thiadiazole

3-(4-chlorobenzoyl)-2-ethoxycarbonyl-2,3-dihydro-2-methyl-5-phenylthio-1,3,4-thiadiazole

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 138612-39-2 3-(4-chlorobenzoyl)-2-ethoxycarbonyl-2,3-dihydro-2-methyl-5-methylthio-1,3,4-thiadiazole

Send

Send

Metric Ton KG G Pound L ML

Send

Send