9-(4-ethoxyphenyl)-4-methyl-7-tosyl-7,8-dihydro-4,7-phenanthrolin-3(4H)-one

Base Information

Chemical Name:9-(4-ethoxyphenyl)-4-methyl-7-tosyl-7,8-dihydro-4,7-phenanthrolin-3(4H)-one
CAS No.:1629780-41-1
Molecular Formula:C₂₈H₂₆N₂O₄S
Molecular Weight:486.591
Hs Code.:

Synonyms:9-(4-ethoxyphenyl)-4-methyl-7-tosyl-7,8-dihydro-4,7-phenanthrolin-3(4H)-one

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Chemical Property of 9-(4-ethoxyphenyl)-4-methyl-7-tosyl-7,8-dihydro-4,7-phenanthrolin-3(4H)-one

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Technology Process of 9-(4-ethoxyphenyl)-4-methyl-7-tosyl-7,8-dihydro-4,7-phenanthrolin-3(4H)-one

There total 3 articles about 9-(4-ethoxyphenyl)-4-methyl-7-tosyl-7,8-dihydro-4,7-phenanthrolin-3(4H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1629780-28-4
N-[3-(4-ethoxyphenyl)prop-2-yn-1-yl]-4-methyl-N-(1-methyl-2-oxo-1,2-dihydroquinolin-6-yl)benzenesulfonamide

: 1629780-41-1
9-(4-ethoxyphenyl)-4-methyl-7-tosyl-7,8-dihydro-4,7-phenanthrolin-3(4H)-one

Guidance literature:: With iron(III) chloride; In acetonitrile; at 80 ℃; for 12h; Inert atmosphere;
DOI:10.1055/s-0033-1340902

Reference yield:

: 699-08-1
1-ethoxy-4-iodobenzene

: 1264630-54-7
C₁₉H₁₅NO₄S

: 1629780-41-1
9-(4-ethoxyphenyl)-4-methyl-7-tosyl-7,8-dihydro-4,7-phenanthrolin-3(4H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / N,N-dimethyl-formamide / 1 h / 20 °C

2: iron(III) chloride / acetonitrile / 12 h / 80 °C / Inert atmosphere

With iron(III) chloride; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1055/s-0033-1340902

Reference yield:

: 92856-41-2
6-(N-tosylamino)coumarin

: 1629780-41-1
9-(4-ethoxyphenyl)-4-methyl-7-tosyl-7,8-dihydro-4,7-phenanthrolin-3(4H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; sodium iodide / acetone / 6 h / Reflux

2: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / N,N-dimethyl-formamide / 1 h / 20 °C

3: iron(III) chloride / acetonitrile / 12 h / 80 °C / Inert atmosphere

With iron(III) chloride; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; triethylamine; sodium iodide; In N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1055/s-0033-1340902