N-<(R)-2-benzyloxypropionyl>-L-phenylalanyl-α-azaproline tert-butyl ester

Base Information

Chemical Name:N-<(R)-2-benzyloxypropionyl>-L-phenylalanyl-α-azaproline tert-butyl ester
CAS No.:159174-59-1
Molecular Formula:C₂₇H₃₅N₃O₅
Molecular Weight:481.592
Hs Code.:

Synonyms:N-<(R)-2-benzyloxypropionyl>-L-phenylalanyl-α-azaproline tert-butyl ester

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Chemical Property of N-<(R)-2-benzyloxypropionyl>-L-phenylalanyl-α-azaproline tert-butyl ester

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Technology Process of N-<(R)-2-benzyloxypropionyl>-L-phenylalanyl-α-azaproline tert-butyl ester

There total 4 articles about N-<(R)-2-benzyloxypropionyl>-L-phenylalanyl-α-azaproline tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 100836-85-9
(R)-2-benzyloxypropionic acid

: 159174-60-4
L-phenylalanyl-α-azaproline tert-butyl ester

: 159174-59-1
N-<(R)-2-benzyloxypropionyl>-L-phenylalanyl-α-azaproline tert-butyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; 1.) 0 deg C, 4 h, 2.) 5 deg C, 16 h;

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 159174-59-1
N-<(R)-2-benzyloxypropionyl>-L-phenylalanyl-α-azaproline tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / DCC / tetrahydrofuran / 1.) 0 deg C, 4 h, 2.) 5 deg C, 16 h

2: 3.2 g / H₂ / 10percent Pd on charcoal / H₂O; methanol / 3 h

3: 86 percent / DCC / tetrahydrofuran; methanol / 1.) 0 deg C, 4 h, 2.) 5 deg C, 16 h

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; water;

Reference yield:

: 159174-58-0
N-benzyloxycarbonyl-L-phenylalanyl-α-azaproline tert-butyl ester

: 159174-59-1
N-<(R)-2-benzyloxypropionyl>-L-phenylalanyl-α-azaproline tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 3.2 g / H₂ / 10percent Pd on charcoal / H₂O; methanol / 3 h

2: 86 percent / DCC / tetrahydrofuran; methanol / 1.) 0 deg C, 4 h, 2.) 5 deg C, 16 h

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; water;