C₃₄H₄₃ClO₄Si

Base Information

• Chemical Name: C₃₄H₄₃ClO₄Si
• CAS No.: 1192815-37-4
• Molecular Formula: C₃₄H₄₃ClO₄Si
• Molecular Weight: 579.252
• Mol file: 1192815-37-4.mol

Synonyms:C₃₄H₄₃ClO₄Si

Chemical Property of C₃₄H₄₃ClO₄Si

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₃₄H₄₃ClO₄Si

There total 2 articles about C₃₄H₄₃ClO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-oxobutyl benzoate (22927-31-7) + (R)-tert-butyl((4-chloro-6-iodohept-6-en-1-yl)oxy)diphenylsilane (1191268-95-7) → C34H43ClO4Si (1192815-37-4)

Guidance literature:

With chromium dichloride; manganese; zirconocene dichloride; 2.9-dimethyl-1,10-phenanthroline; C₂₆H₃₂Cl₂N₂O₄S; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; lithium chloride; In acetonitrile; at 20 ℃; for 10h; optical yield given as %de; Inert atmosphere;

DOI:10.1021/ja9058475

Reference yield:

4-oxobutyl benzoate (22927-31-7) + (R)-tert-butyl((4-chloro-6-iodohept-6-en-1-yl)oxy)diphenylsilane (1191268-95-7) → C34H43ClO4Si (1192815-37-4) + C34H43ClO4Si (1192815-38-5)

Guidance literature:

With chromium dichloride; manganese; zirconocene dichloride; DMP*NiCl₂ dimer; C₁₄H₂₀N₂O₄S; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; lithium chloride; In acetonitrile; optical yield given as %de; Inert atmosphere;

DOI:10.1021/ja905843e

Reference yield: 88.0%

C34H43ClO4Si (1192815-37-4) → C34H42O4Si (481048-26-4)

Guidance literature:

With 18-crown-6 ether; potassium hydride; In toluene; mineral oil; at -78 - -20 ℃; optical yield given as %de; Inert atmosphere;

DOI:10.1021/ja9058475

upstream raw materials:

4-oxobutyl benzoate

(R)-tert-butyl((4-chloro-6-iodohept-6-en-1-yl)oxy)diphenylsilane

Downstream raw materials:

C₃₄H₄₂O₄Si