3-(3',5'-Dibromo-2'-methoxyphenyl)-2-formamido-2-propenoic Acid Methyl Ester

Base Information

Chemical Name:3-(3',5'-Dibromo-2'-methoxyphenyl)-2-formamido-2-propenoic Acid Methyl Ester
CAS No.:133886-89-2
Molecular Formula:C₁₂H₁₁Br₂NO₄
Molecular Weight:393.032
Hs Code.:

Synonyms:3-(3',5'-Dibromo-2'-methoxyphenyl)-2-formamido-2-propenoic Acid Methyl Ester

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Chemical Property of 3-(3',5'-Dibromo-2'-methoxyphenyl)-2-formamido-2-propenoic Acid Methyl Ester

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Technology Process of 3-(3',5'-Dibromo-2'-methoxyphenyl)-2-formamido-2-propenoic Acid Methyl Ester

There total 1 articles about 3-(3',5'-Dibromo-2'-methoxyphenyl)-2-formamido-2-propenoic Acid Methyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 61657-65-6
3,5-dibromo-2-methoxybenzaldehyde

: 39687-95-1
isocyanoacetic acid methyl ester

: 133886-89-2
3-(3',5'-Dibromo-2'-methoxyphenyl)-2-formamido-2-propenoic Acid Methyl Ester

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; for 12h; Ambient temperature;

Reference yield: 80.0%

: 133886-89-2
3-(3',5'-Dibromo-2'-methoxyphenyl)-2-formamido-2-propenoic Acid Methyl Ester

: 133871-72-4
3-(3',5'-Dibromo-2'-methoxyphenyl)-2-isocyano-2-propenoic Acid Methyl Ester

Guidance literature:: With triethylamine; trichlorophosphate; In dichloromethane; for 3h; Ambient temperature;

Reference yield:

: 133886-89-2
3-(3',5'-Dibromo-2'-methoxyphenyl)-2-formamido-2-propenoic Acid Methyl Ester

: 133871-80-4
3-(3',5'-Dibromo-2'-methoxyphenyl)-1H-pyrrole

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / triethylamine, phosphoryl chloride / CH₂Cl₂ / 3 h / Ambient temperature

2: 37 percent / n-butyllithium / tetrahydrofuran; pentane / 1 h / Ambient temperature

3: 68 percent / 1M KOH / methanol; H₂O / 96 h / Heating

4: 26 percent / Cu / quinoline / 180 - 190 °C

With potassium hydroxide; n-butyllithium; copper; triethylamine; trichlorophosphate; In tetrahydrofuran; quinoline; methanol; dichloromethane; water; pentane;