allyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-benzamido-2-deoxy-β-D-glucopyranosyl)-α-D-galactopyranoside

Base Information

• Chemical Name: allyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-benzamido-2-deoxy-β-D-glucopyranosyl)-α-D-galactopyranoside
• CAS No.: 72348-55-1
• Molecular Formula: C₄₉H₅₅NO₁₄
• Molecular Weight: 881.974

Synonyms:allyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-benzamido-2-deoxy-β-D-glucopyranosyl)-α-D-galactopyranoside

Chemical Property of allyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-benzamido-2-deoxy-β-D-glucopyranosyl)-α-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of allyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-benzamido-2-deoxy-β-D-glucopyranosyl)-α-D-galactopyranoside

There total 4 articles about allyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-benzamido-2-deoxy-β-D-glucopyranosyl)-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

1,2,4,6-tetra-O-acetyl-2-benzamido-2-deoxy-β-D-glucopyranose (10385-49-6,14086-92-1) + allyl 2,3,6-tri-O-benzyl-α-D-galactopyranoside (61893-74-1) → allyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-benzamido-2-deoxy-β-D-glucopyranosyl)-α-D-galactopyranoside (72348-55-1)

Guidance literature:

With calcium sulfate; iron(III) chloride; tetramethylurea; In dichloromethane; at 35 ℃;

DOI:10.1016/0008-6215(85)85205-8

Reference yield:

benzoyl chloride (98-88-4) → allyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-benzamido-2-deoxy-β-D-glucopyranosyl)-α-D-galactopyranoside (72348-55-1)

Guidance literature:

Multi-step reaction with 2 steps

2: 30 percent / FeCl₃, CaSO₄, tetramethylurea / CH₂Cl₂ / 35 °C

With calcium sulfate; iron(III) chloride; tetramethylurea; In dichloromethane;

DOI:10.1016/0008-6215(85)85205-8

Reference yield:

tetra-acetyl glucosamine (17460-45-6,23707-23-5,23739-93-7,23743-51-3,26108-75-8,59042-16-9,124516-07-0,124580-56-9) → allyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-benzamido-2-deoxy-β-D-glucopyranosyl)-α-D-galactopyranoside (72348-55-1)

Guidance literature:

Multi-step reaction with 2 steps

2: 30 percent / FeCl₃, CaSO₄, tetramethylurea / CH₂Cl₂ / 35 °C

With calcium sulfate; iron(III) chloride; tetramethylurea; In dichloromethane;

DOI:10.1016/0008-6215(85)85205-8

upstream raw materials:

1,2,4,6-tetra-O-acetyl-2-benzamido-2-deoxy-β-D-glucopyranose

allyl 2,3,6-tri-O-benzyl-α-D-galactopyranoside

benzoyl chloride

tetra-acetyl glucosamine

Downstream raw materials:

allyl O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-(1->4)-2,4,6-tri-O-benzyl-α-D-galactopyranoside

allyl 4-O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranoyl)-2,3,6-tri-O-benzyl-α-D-galactopyranoside

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