{[(di-tert-butylphosphanyl)(phenyl)amino]methylene}diisopropylammonium trifluoromethanesulfonate

Base Information

Chemical Name:{[(di-tert-butylphosphanyl)(phenyl)amino]methylene}diisopropylammonium trifluoromethanesulfonate
CAS No.:1569096-91-8
Molecular Formula:CF₃O₃S*C₂₁H₃₈N₂P
Molecular Weight:498.59
Hs Code.:

Synonyms:{[(di-tert-butylphosphanyl)(phenyl)amino]methylene}diisopropylammonium trifluoromethanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {[(di-tert-butylphosphanyl)(phenyl)amino]methylene}diisopropylammonium trifluoromethanesulfonate

Chemical Property:

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Technology Process of {[(di-tert-butylphosphanyl)(phenyl)amino]methylene}diisopropylammonium trifluoromethanesulfonate

There total 6 articles about {[(di-tert-butylphosphanyl)(phenyl)amino]methylene}diisopropylammonium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1569096-89-4
{[(di-tert-butylphosphoroselenoyl)(phenyl)amino]methylene}-diisopropylammonium trifluoromethanesulfonate

: 1569096-91-8
{[(di-tert-butylphosphanyl)(phenyl)amino]methylene}diisopropylammonium trifluoromethanesulfonate

Guidance literature:: With Hexamethylphosphorous triamide; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/ejic.201301365

Reference yield:

: 56898-62-5
P,P-di-tert-butyl-N-phenylphosphinoselenoic amide

: 1569096-91-8
{[(di-tert-butylphosphanyl)(phenyl)amino]methylene}diisopropylammonium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 3 h / 0 - 20 °C

2: Hexamethylphosphorous triamide / dichloromethane / 0.5 h / 20 °C

With Hexamethylphosphorous triamide; In dichloromethane;
DOI:10.1002/ejic.201402166

Reference yield:

: 62-53-3
aniline

: 1569096-91-8
{[(di-tert-butylphosphanyl)(phenyl)amino]methylene}diisopropylammonium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / 1.5 h / 20 °C / Reflux; Inert atmosphere

2: dichloromethane / 3 h / 20 °C / Inert atmosphere

3: Hexamethylphosphorous triamide / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

With triethylamine; Hexamethylphosphorous triamide; In dichloromethane;
DOI:10.1002/ejic.201301365