{[(di-tert-butylphosphoroselenoyl)(phenyl)amino]methylene}-diisopropylammonium trifluoromethanesulfonate

Base Information

Chemical Name:{[(di-tert-butylphosphoroselenoyl)(phenyl)amino]methylene}-diisopropylammonium trifluoromethanesulfonate
CAS No.:1569096-89-4
Molecular Formula:CF₃O₃S*C₂₁H₃₈N₂PSe
Molecular Weight:577.55
Hs Code.:

Synonyms:{[(di-tert-butylphosphoroselenoyl)(phenyl)amino]methylene}-diisopropylammonium trifluoromethanesulfonate

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Chemical Property of {[(di-tert-butylphosphoroselenoyl)(phenyl)amino]methylene}-diisopropylammonium trifluoromethanesulfonate

Chemical Property:

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Technology Process of {[(di-tert-butylphosphoroselenoyl)(phenyl)amino]methylene}-diisopropylammonium trifluoromethanesulfonate

There total 4 articles about {[(di-tert-butylphosphoroselenoyl)(phenyl)amino]methylene}-diisopropylammonium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 56898-62-5
P,P-di-tert-butyl-N-phenylphosphinoselenoic amide

: 1,1,5,5-Tetraisopropyl-1,5-diazonia-3-oxapent-1,4-dienyl bis(trifluoromethanesulfonate)

: 1569096-89-4
{[(di-tert-butylphosphoroselenoyl)(phenyl)amino]methylene}-diisopropylammonium trifluoromethanesulfonate

Guidance literature:: In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/ejic.201301365

Reference yield:

: 39106-95-1
di-tert-butylphosphanylbromide

: 1569096-89-4
{[(di-tert-butylphosphoroselenoyl)(phenyl)amino]methylene}-diisopropylammonium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / 1.5 h / 20 °C / Reflux; Inert atmosphere

2: dichloromethane / 3 h / 20 °C / Inert atmosphere

With triethylamine; In dichloromethane;
DOI:10.1002/ejic.201301365

Reference yield:

: 62-53-3
aniline

: 1569096-89-4
{[(di-tert-butylphosphoroselenoyl)(phenyl)amino]methylene}-diisopropylammonium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / 1.5 h / 20 °C / Reflux; Inert atmosphere

2: dichloromethane / 3 h / 20 °C / Inert atmosphere

With triethylamine; In dichloromethane;
DOI:10.1002/ejic.201301365