Technology Process of C13H10BrFO2
There total 7 articles about C13H10BrFO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water; sodium hydroxide;
In
tetrahydrofuran;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium carbonate / N,N-dimethyl-formamide / 80 °C / Inert atmosphere
2: palladium on activated charcoal; hydrogen / ethyl acetate / 20 °C
3: tert.-butylnitrite; copper(ll) bromide / acetonitrile / -10 °C
4: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 70 °C
5: N,N-dimethyl-formamide / 5 h / 70 °C
6: sodium hydroxide; water / tetrahydrofuran / 20 °C
With
N-Bromosuccinimide; tert.-butylnitrite; palladium on activated charcoal; water; hydrogen; potassium carbonate; sodium hydroxide; copper(ll) bromide; dibenzoyl peroxide;
In
tetrahydrofuran; tetrachloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: palladium on activated charcoal; hydrogen / ethyl acetate / 20 °C
2: tert.-butylnitrite; copper(ll) bromide / acetonitrile / -10 °C
3: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 70 °C
4: N,N-dimethyl-formamide / 5 h / 70 °C
5: sodium hydroxide; water / tetrahydrofuran / 20 °C
With
N-Bromosuccinimide; tert.-butylnitrite; palladium on activated charcoal; water; hydrogen; sodium hydroxide; copper(ll) bromide; dibenzoyl peroxide;
In
tetrahydrofuran; tetrachloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;