methyl 2-(4-(2-(3,5-dimethylisoxazol-4-yl)-2-hydroxyethoxy)phenyl)acetate

Base Information

Chemical Name:methyl 2-(4-(2-(3,5-dimethylisoxazol-4-yl)-2-hydroxyethoxy)phenyl)acetate
CAS No.:1421838-38-1
Molecular Formula:C₁₆H₁₉NO₅
Molecular Weight:305.331
Hs Code.:

Synonyms:methyl 2-(4-(2-(3,5-dimethylisoxazol-4-yl)-2-hydroxyethoxy)phenyl)acetate

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Chemical Property of methyl 2-(4-(2-(3,5-dimethylisoxazol-4-yl)-2-hydroxyethoxy)phenyl)acetate

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Technology Process of methyl 2-(4-(2-(3,5-dimethylisoxazol-4-yl)-2-hydroxyethoxy)phenyl)acetate

There total 9 articles about methyl 2-(4-(2-(3,5-dimethylisoxazol-4-yl)-2-hydroxyethoxy)phenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1421838-37-0
methyl 2-(4-(2-(3,5-dimethylisoxazol-4-yl)-2-oxoethoxy)phenyl)acetate

: 1421838-38-1
methyl 2-(4-(2-(3,5-dimethylisoxazol-4-yl)-2-hydroxyethoxy)phenyl)acetate

Guidance literature:: With sodium tetrahydroborate; In methanol; at 20 ℃; for 1h;

Reference yield:

: 2510-36-3
3,5-dimethyl-4-isoxazolecarboxylic acid

: 1421838-38-1
methyl 2-(4-(2-(3,5-dimethylisoxazol-4-yl)-2-hydroxyethoxy)phenyl)acetate

Guidance literature:: Multi-step reaction with 8 steps

1: thionyl chloride / 70 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

3: Dess-Martin periodane / dichloromethane / 1.17 h / 0 - 20 °C

4: tetrahydrofuran; diethyl ether / 1.67 h / 0 - 20 °C

5: pyridinium chlorochromate / dichloromethane / 1 h / 0 - 20 °C

6: bromine; acetic acid / tetrachloromethane / 0.33 h / 48 °C

7: potassium carbonate / acetonitrile / 1.5 h / 20 °C

8: sodium tetrahydroborate / methanol / 1 h / 20 °C

With sodium tetrahydroborate; lithium aluminium tetrahydride; thionyl chloride; bromine; potassium carbonate; Dess-Martin periodane; acetic acid; pyridinium chlorochromate; In tetrahydrofuran; methanol; tetrachloromethane; diethyl ether; dichloromethane; acetonitrile;

Reference yield:

: 156-38-7
4-hydroxyphenylacetate

: 1421838-38-1
methyl 2-(4-(2-(3,5-dimethylisoxazol-4-yl)-2-hydroxyethoxy)phenyl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / 2 h / 0 °C

2: potassium carbonate / acetonitrile / 1.5 h / 20 °C

3: sodium tetrahydroborate / methanol / 1 h / 20 °C

With hydrogenchloride; sodium tetrahydroborate; potassium carbonate; In methanol; acetonitrile;