N-(5-Methoxy-2,3-dihydro-1H-inden-1-ylidene)hydroxylamine

Base Information

Chemical Name:N-(5-Methoxy-2,3-dihydro-1H-inden-1-ylidene)hydroxylamine
CAS No.:90921-94-1
Molecular Formula:C10H11 N O2
Molecular Weight:177.203
Hs Code.:
NSC Number:148925
DSSTox Substance ID:DTXSID90419304

Synonyms:90921-94-1;NSC148925;SCHEMBL16082212;DTXSID90419304;NSC-148925;N-(5-Methoxy-2,3-dihydro-1H-inden-1-ylidene)hydroxylamine

Suppliers and Price of N-(5-Methoxy-2,3-dihydro-1H-inden-1-ylidene)hydroxylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of N-(5-Methoxy-2,3-dihydro-1H-inden-1-ylidene)hydroxylamine

Chemical Property:

Vapor Pressure:2.24E-05mmHg at 25°C
Boiling Point:346°Cat760mmHg
Flash Point:163.1°C
Density:1.22g/cm³
XLogP3:1.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:177.078978594
Heavy Atom Count:13
Complexity:215

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC2=C(C=C1)C(=NO)CC2
Isomeric SMILES:COC1=CC2=C(C=C1)/C(=N\O)/CC2

Technology Process of N-(5-Methoxy-2,3-dihydro-1H-inden-1-ylidene)hydroxylamine

There total 4 articles about N-(5-Methoxy-2,3-dihydro-1H-inden-1-ylidene)hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 5111-70-6
5-methoxy-1-indanone

: 90921-94-1
5-methoxy-1-indanone oxime

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In methanol; at 22 ℃; for 16h;

Reference yield:

: 3470-49-3
5-hydroxy-2,3-dihydro-1H-indene-1-one

: 90921-94-1
5-methoxy-1-indanone oxime

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 h / 20 °C / Inert atmosphere

2: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 4 h / Reflux; Inert atmosphere

With hydroxylamine hydrochloride; sodium acetate; potassium carbonate; In ethanol; water; N,N-dimethyl-formamide;