N¹-(5-methyl-2-nitrophenyl)-N²-[α-chloro-(4-methoxybenzylidene)]hydrazide

Base Information

Chemical Name:N¹-(5-methyl-2-nitrophenyl)-N²-[α-chloro-(4-methoxybenzylidene)]hydrazide
CAS No.:872311-85-8
Molecular Formula:C₁₅H₁₄ClN₃O₃
Molecular Weight:319.747
Hs Code.:

N<sup>1</sup>-(5-methyl-2-nitrophenyl)-N<sup>2</sup>-[α-chloro-(4-methoxybenzylidene)]hydrazide

Synonyms:N¹-(5-methyl-2-nitrophenyl)-N²-[α-chloro-(4-methoxybenzylidene)]hydrazide

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Chemical Property of N¹-(5-methyl-2-nitrophenyl)-N²-[α-chloro-(4-methoxybenzylidene)]hydrazide

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Technology Process of N¹-(5-methyl-2-nitrophenyl)-N²-[α-chloro-(4-methoxybenzylidene)]hydrazide

There total 3 articles about N¹-(5-methyl-2-nitrophenyl)-N²-[α-chloro-(4-methoxybenzylidene)]hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 872311-86-9
N¹-(5-methyl-2-nitrophenyl)-N²-(4-methoxybenzoyl)hydrazide

: 872311-85-8
N¹-(5-methyl-2-nitrophenyl)-N²-[α-chloro-(4-methoxybenzylidene)]hydrazide

Guidance literature:: With trichlorophosphate; for 1h; Heating;
DOI:10.1021/jm0504149

Reference yield:

: 100-07-2
4-methoxy-benzoyl chloride

: 872311-85-8
N¹-(5-methyl-2-nitrophenyl)-N²-[α-chloro-(4-methoxybenzylidene)]hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / pyridine / 1 h / Heating

2: 60 percent / POCl₃ / 1 h / Heating

With pyridine; trichlorophosphate;
DOI:10.1021/jm0504149

Reference yield:

: 56637-42-4
5-methyl-2-nitrophenylhydrazine

: 872311-85-8
N¹-(5-methyl-2-nitrophenyl)-N²-[α-chloro-(4-methoxybenzylidene)]hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / pyridine / 1 h / Heating

2: 60 percent / POCl₃ / 1 h / Heating

With pyridine; trichlorophosphate;
DOI:10.1021/jm0504149