Technology Process of C56H75N7O17S
There total 3 articles about C56H75N7O17S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(II) sulfate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
water; dimethyl sulfoxide;
at 40 ℃;
for 48h;
DOI:10.1021/ol400401d
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: dicyclohexyl-carbodiimide / dichloromethane / 0.08 h / 0 °C / Inert atmosphere
1.2: 48 h / 20 °C / Inert atmosphere
2.1: tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; sodium L-ascorbate; copper(II) sulfate / dimethyl sulfoxide; water / 48 h / 40 °C
With
copper(II) sulfate; sodium L-ascorbate; dicyclohexyl-carbodiimide; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
dichloromethane; water; dimethyl sulfoxide;
2.1: |Huisgen Cycloaddition;
DOI:10.1021/ol400401d
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: water; potassium hydroxide / methanol / 2.5 h / 50 °C
2.1: dicyclohexyl-carbodiimide / dichloromethane / 0.08 h / 0 °C / Inert atmosphere
2.2: 48 h / 20 °C / Inert atmosphere
3.1: tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; sodium L-ascorbate; copper(II) sulfate / dimethyl sulfoxide; water / 48 h / 40 °C
With
water; copper(II) sulfate; sodium L-ascorbate; dicyclohexyl-carbodiimide; potassium hydroxide; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
methanol; dichloromethane; water; dimethyl sulfoxide;
3.1: |Huisgen Cycloaddition;
DOI:10.1021/ol400401d
