(4S,2E)-4-hydroxy-3-methyl-4-[(1S,6S)-3-methyl-2-oxo-6-(prop-1-en-2-yl)cyclohex-3-enyl]but-2-enyl acetate

Base Information

Chemical Name:(4S,2E)-4-hydroxy-3-methyl-4-[(1S,6S)-3-methyl-2-oxo-6-(prop-1-en-2-yl)cyclohex-3-enyl]but-2-enyl acetate
CAS No.:1207372-65-3
Molecular Formula:C₁₇H₂₄O₄
Molecular Weight:292.375
Hs Code.:

Synonyms:(4S,2E)-4-hydroxy-3-methyl-4-[(1S,6S)-3-methyl-2-oxo-6-(prop-1-en-2-yl)cyclohex-3-enyl]but-2-enyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S,2E)-4-hydroxy-3-methyl-4-[(1S,6S)-3-methyl-2-oxo-6-(prop-1-en-2-yl)cyclohex-3-enyl]but-2-enyl acetate

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Technology Process of (4S,2E)-4-hydroxy-3-methyl-4-[(1S,6S)-3-methyl-2-oxo-6-(prop-1-en-2-yl)cyclohex-3-enyl]but-2-enyl acetate

There total 1 articles about (4S,2E)-4-hydroxy-3-methyl-4-[(1S,6S)-3-methyl-2-oxo-6-(prop-1-en-2-yl)cyclohex-3-enyl]but-2-enyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 26586-02-7
(E)-4-acetoxy-2-methylcrotonaldehyde

: 2244-16-8,6485-40-1
(S)-p-mentha-6,8-dien-2-one

: 1207372-65-3
(4S,2E)-4-hydroxy-3-methyl-4-[(1S,6S)-3-methyl-2-oxo-6-(prop-1-en-2-yl)cyclohex-3-enyl]but-2-enyl acetate

: 1207372-44-8
(4R,2E)-4-hydroxy-3-methyl-4-[(1S,6S)-3-methyl-2-oxo-6-(prop-1-en-2-yl)cyclohex-3-enyl]but-2-enyl acetate

Guidance literature:: (S)-p-mentha-6,8-dien-2-one; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

(E)-4-acetoxy-2-methylcrotonaldehyde; In tetrahydrofuran; at -78 ℃; for 3h; optical yield given as %de; Inert atmosphere;
DOI:10.1055/s-0029-1216990