2R-[(2R-acetylamino-3-tritylsulfanyl-propionyl)-(methyl)-amino]-3-mercapto-propionic acid methyl ester

Base Information

• Chemical Name: 2R-[(2R-acetylamino-3-tritylsulfanyl-propionyl)-(methyl)-amino]-3-mercapto-propionic acid methyl ester
• CAS No.: 1129670-85-4
• Molecular Formula: C₂₉H₃₂N₂O₄S₂
• Molecular Weight: 536.716

Synonyms:2R-[(2R-acetylamino-3-tritylsulfanyl-propionyl)-(methyl)-amino]-3-mercapto-propionic acid methyl ester

Chemical Property of 2R-[(2R-acetylamino-3-tritylsulfanyl-propionyl)-(methyl)-amino]-3-mercapto-propionic acid methyl ester

Chemical Property:

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Technology Process of 2R-[(2R-acetylamino-3-tritylsulfanyl-propionyl)-(methyl)-amino]-3-mercapto-propionic acid methyl ester

There total 1 articles about 2R-[(2R-acetylamino-3-tritylsulfanyl-propionyl)-(methyl)-amino]-3-mercapto-propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

2R-[(2R-acetylamino-3-tritylsulfanyl-propionyl)-(methyl)-amino]-3-tert-butyldisulfanyl-propionic acid methyl ester (1129670-83-2) → 2R-[(2R-acetylamino-3-tritylsulfanyl-propionyl)-(methyl)-amino]-3-mercapto-propionic acid methyl ester (1129670-85-4)

Guidance literature:

With 4-methyl-morpholine; D,L-dithiothreitol; In N,N-dimethyl-formamide; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1016/j.tet.2008.11.085

Reference yield:

2R-[(2R-acetylamino-3-tritylsulfanyl-propionyl)-(methyl)-amino]-3-mercapto-propionic acid methyl ester (1129670-85-4) + 5,5'-dinitro-2,2'-disulfanediyl-bis-pyridine (2127-10-8) → C34H34N4O6S3

Guidance literature:

In dichloromethane; at 20 ℃; for 14h; Inert atmosphere;

DOI:10.1016/j.tet.2008.11.085

upstream raw materials:

2R-[(2R-acetylamino-3-tritylsulfanyl-propionyl)-(methyl)-amino]-3-tert-butyldisulfanyl-propionic acid methyl ester

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