1′-(di-tert-butylphosphinoselenoyl)-1-(diphenylphosphinoselenoyl)ferrocene

Base Information

Chemical Name:1′-(di-tert-butylphosphinoselenoyl)-1-(diphenylphosphinoselenoyl)ferrocene
CAS No.:1137724-61-8
Molecular Formula:C₃₀H₃₆FeP₂Se₂
Molecular Weight:672.33
Hs Code.:

Synonyms:1′-(di-tert-butylphosphinoselenoyl)-1-(diphenylphosphinoselenoyl)ferrocene

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Chemical Property of 1′-(di-tert-butylphosphinoselenoyl)-1-(diphenylphosphinoselenoyl)ferrocene

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Technology Process of 1′-(di-tert-butylphosphinoselenoyl)-1-(diphenylphosphinoselenoyl)ferrocene

There total 3 articles about 1′-(di-tert-butylphosphinoselenoyl)-1-(diphenylphosphinoselenoyl)ferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.3%

: 7782-49-2
selenium

: 95408-38-1
1-(diphenylphosphino)ferrocene-1-(di-tert-butylphosphino)ferrocene

: 1137724-61-8
1′-(di-tert-butylphosphinoselenoyl)-1-(diphenylphosphinoselenoyl)ferrocene

Guidance literature:: In chloroform; (Ar); std. Schlenk technique; CHCl3 was added to mixt. of Se (2 equiv.) and Fe complex; refluxed overnight; cooled; filtered; concd. (vac.); MeOH added; kept in refrigerator overnight; filtered; washed (Et2O); dried (vac.); elem. anal.;
DOI:10.1021/om800850c

Reference yield: 20.9%

: 7782-49-2
selenium

: 95408-38-1
1-(diphenylphosphino)ferrocene-1-(di-tert-butylphosphino)ferrocene

: 1137724-64-1
[((C₆H₅)2PC₅H₄)Fe(C₅H₄P(Se)(C(CH₃)3)2)]

: 1137724-61-8
1′-(di-tert-butylphosphinoselenoyl)-1-(diphenylphosphinoselenoyl)ferrocene

Guidance literature:: In toluene; (Ar); std. Schlenk technique; Se (1 equiv.) and Fe complex were combined; cooled to 0°C; toluene was added; stirred at 0°C for 4 h; evapd. (vac.); chromd. (silica gel, hexane/toluene, 1/1); solvent removed; elem. anal.;
DOI:10.1021/om800850c