1-(2,4-dichlorophenyl)-6-phenylpyridazin-4(1H)-one

Base Information

• Chemical Name: 1-(2,4-dichlorophenyl)-6-phenylpyridazin-4(1H)-one
• CAS No.: 6533-31-9
• Molecular Formula: C₁₉H₂₄ClN₂O₃P
• Molecular Weight: 394.838

Synonyms:1,3,2-Diazaphosphorine,2-chlorohexahydro-1,3-bis(p-methoxybenzyl)-, 2-oxide (7CI,8CI); NSC 79565

Chemical Property of 1-(2,4-dichlorophenyl)-6-phenylpyridazin-4(1H)-one

Chemical Property:

• Vapor Pressure: 2.93E-09mmHg at 25°C
• Boiling Point: 533.9°Cat760mmHg
• Flash Point: 276.7°C
• Density: 1.28g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(2,4-dichlorophenyl)-6-phenylpyridazin-4(1H)-one

There total 1 articles about 1-(2,4-dichlorophenyl)-6-phenylpyridazin-4(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N(1),N(3)-3-bis(4-methoxybenzyl)propane-1,3-diamine (59211-76-6) → 2-chloro-1,3-bis-(4-methoxy-benzyl)-[1,3,2]diazaphosphinane 2-oxide (6533-31-9)

Guidance literature:

With triethylamine; trichlorophosphate; In diethyl ether;

DOI:10.1021/jm00323a034

Reference yield:

piperidine (110-89-4) + 2-chloro-1,3-bis-(4-methoxy-benzyl)-[1,3,2]diazaphosphinane 2-oxide (6533-31-9) → 1,3-bis-(4-methoxy-benzyl)-2-piperidin-1-yl-[1,3,2]diazaphosphinane 2-oxide (14757-30-3)

Guidance literature:

With triethylamine; In benzene; Heating;

DOI:10.1021/jm00315a044

Reference yield:

2-chloro-1,3-bis-(4-methoxy-benzyl)-[1,3,2]diazaphosphinane 2-oxide (6533-31-9) + diethylamine (109-89-7) → [1,3-bis-(4-methoxy-benzyl)-2-oxo-2λ5-[1,3,2]diazaphosphinan-2-yl]-diethyl-amine (13348-65-7)

Guidance literature:

With triethylamine; In benzene; Heating;

DOI:10.1021/jm00315a044

upstream raw materials:

N⁽¹⁾,N⁽³⁾-3-bis(4-methoxybenzyl)propane-1,3-diamine

Downstream raw materials:

1,3-bis-(4-methoxy-benzyl)-2-piperidin-1-yl-[1,3,2]diazaphosphinane 2-oxide

[1,3-bis-(4-methoxy-benzyl)-2-oxo-2λ⁵-[1,3,2]diazaphosphinan-2-yl]-diethyl-amine

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