benzyl 4-O-(methyl β-D-glucopyranosyluronate)-2-benzyloxy-6-pentadecanylbenzoate

Base Information

Chemical Name:benzyl 4-O-(methyl β-D-glucopyranosyluronate)-2-benzyloxy-6-pentadecanylbenzoate
CAS No.:869996-30-5
Molecular Formula:C₄₃H₅₈O₁₀
Molecular Weight:734.928
Hs Code.:

Synonyms:benzyl 4-O-(methyl β-D-glucopyranosyluronate)-2-benzyloxy-6-pentadecanylbenzoate

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Chemical Property of benzyl 4-O-(methyl β-D-glucopyranosyluronate)-2-benzyloxy-6-pentadecanylbenzoate

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Technology Process of benzyl 4-O-(methyl β-D-glucopyranosyluronate)-2-benzyloxy-6-pentadecanylbenzoate

There total 11 articles about benzyl 4-O-(methyl β-D-glucopyranosyluronate)-2-benzyloxy-6-pentadecanylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 869996-29-2
benzyl 4-O-(methyl 2',3',4'-tri-O-acetyl-β-D-glucopyranosyluronate)-2-benzyloxy-6-pentadecanylbenzoate

: 869996-30-5
benzyl 4-O-(methyl β-D-glucopyranosyluronate)-2-benzyloxy-6-pentadecanylbenzoate

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 0.333333h;
DOI:10.1021/jo051384k

Reference yield:

: 869996-09-8
2,4-bis(benzyloxy)-6-pentadecanylbenzoic acid

: 869996-30-5
benzyl 4-O-(methyl β-D-glucopyranosyluronate)-2-benzyloxy-6-pentadecanylbenzoate

Guidance literature:: Multi-step reaction with 5 steps

1: 99 percent / H₂ / Pd/C / ethyl acetate / 5 h / 20 °C / 760 Torr

2: 88 percent / KHCO₃ / dimethylformamide / 40 h / Heating

3: Ag₂O / acetonitrile / 6 h / 38 °C

4: 112 mg / K₂CO₃ / acetone / 12 h / Heating

5: 78 percent / K₂CO₃ / methanol / 0.33 h / 20 °C

With hydrogen; potassium carbonate; potassium hydrogencarbonate; silver(l) oxide; palladium on activated charcoal; In methanol; ethyl acetate; N,N-dimethyl-formamide; acetone; acetonitrile; 3: Koenigs-Knorr reaction;
DOI:10.1021/jo051384k

Reference yield:

: 869996-08-7
2,4-bis-benzyloxy-6-pentadecyl-benzoic acid ethyl ester

: 869996-30-5
benzyl 4-O-(methyl β-D-glucopyranosyluronate)-2-benzyloxy-6-pentadecanylbenzoate

Guidance literature:: Multi-step reaction with 6 steps

1: 1.40 g / KOH / dimethylsulfoxide; H₂O / 24 h / 90 °C

2: 99 percent / H₂ / Pd/C / ethyl acetate / 5 h / 20 °C / 760 Torr

3: 88 percent / KHCO₃ / dimethylformamide / 40 h / Heating

4: Ag₂O / acetonitrile / 6 h / 38 °C

5: 112 mg / K₂CO₃ / acetone / 12 h / Heating

6: 78 percent / K₂CO₃ / methanol / 0.33 h / 20 °C

With potassium hydroxide; hydrogen; potassium carbonate; potassium hydrogencarbonate; silver(l) oxide; palladium on activated charcoal; In methanol; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetone; acetonitrile; 4: Koenigs-Knorr reaction;
DOI:10.1021/jo051384k