Hexadecanoic acid (1R,2R,3S,4S,5R,6S)-2,3,4,5-tetrakis-benzyloxy-6-[benzyloxy-((R)-2-hexadecanoyloxy-3-hexanoyloxy-propoxy)-phosphoryloxy]-cyclohexyl ester

Base Information

Chemical Name:Hexadecanoic acid (1R,2R,3S,4S,5R,6S)-2,3,4,5-tetrakis-benzyloxy-6-[benzyloxy-((R)-2-hexadecanoyloxy-3-hexanoyloxy-propoxy)-phosphoryloxy]-cyclohexyl ester
CAS No.:499142-87-9
Molecular Formula:C₈₂H₁₁₉O₁₄P
Molecular Weight:1359.81
Hs Code.:

Hexadecanoic acid (1R,2R,3S,4S,5R,6S)-2,3,4,5-tetrakis-benzyloxy-6-[benzyloxy-((R)-2-hexadecanoyloxy-3-hexanoyloxy-propoxy)-phosphoryloxy]-cyclohexyl ester

Synonyms:Hexadecanoic acid (1R,2R,3S,4S,5R,6S)-2,3,4,5-tetrakis-benzyloxy-6-[benzyloxy-((R)-2-hexadecanoyloxy-3-hexanoyloxy-propoxy)-phosphoryloxy]-cyclohexyl ester

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Chemical Property of Hexadecanoic acid (1R,2R,3S,4S,5R,6S)-2,3,4,5-tetrakis-benzyloxy-6-[benzyloxy-((R)-2-hexadecanoyloxy-3-hexanoyloxy-propoxy)-phosphoryloxy]-cyclohexyl ester

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Technology Process of Hexadecanoic acid (1R,2R,3S,4S,5R,6S)-2,3,4,5-tetrakis-benzyloxy-6-[benzyloxy-((R)-2-hexadecanoyloxy-3-hexanoyloxy-propoxy)-phosphoryloxy]-cyclohexyl ester

There total 9 articles about Hexadecanoic acid (1R,2R,3S,4S,5R,6S)-2,3,4,5-tetrakis-benzyloxy-6-[benzyloxy-((R)-2-hexadecanoyloxy-3-hexanoyloxy-propoxy)-phosphoryloxy]-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Hexadecanoic acid (1R,2R,3S,4S,5R,6S)-2,3,4,5-tetrakis-benzyloxy-6-[benzyloxy-((R)-2-hexadecanoyloxy-3-hexanoyloxy-propoxy)-phosphanyloxy]-cyclohexyl ester

: 499142-87-9
Hexadecanoic acid (1R,2R,3S,4S,5R,6S)-2,3,4,5-tetrakis-benzyloxy-6-[benzyloxy-((R)-2-hexadecanoyloxy-3-hexanoyloxy-propoxy)-phosphoryloxy]-cyclohexyl ester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -40 - 20 ℃;
DOI:10.1021/ol0202161

Reference yield:

: Hexadecanoic acid (1S,2S,3S,4R,5S,6R)-2-allyloxy-3,4,5,6-tetrakis-benzyloxy-cyclohexyl ester

: 499142-87-9
Hexadecanoic acid (1R,2R,3S,4S,5R,6S)-2,3,4,5-tetrakis-benzyloxy-6-[benzyloxy-((R)-2-hexadecanoyloxy-3-hexanoyloxy-propoxy)-phosphoryloxy]-cyclohexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 35 percent / PdCl₂; NaOAc / acetic acid; H₂O / 20 °C

2: 82 percent / N,N-diisopropylammonium tetrazolide / CH₂Cl₂ / 5 h / 20 °C

3: 1H-tetrazole / CH₂Cl₂ / Heating

4: m-chloroperoxybenzoic acid / CH₂Cl₂ / -40 - 20 °C

With 1H-tetrazole; N,N-diisopropylamine tetrazolide; sodium acetate; 3-chloro-benzenecarboperoxoic acid; palladium dichloride; In dichloromethane; water; acetic acid;
DOI:10.1021/ol0202161

Reference yield:

: 24558-77-8
3,4,5,6-tetra-O-benzyl inositol

: 499142-87-9
Hexadecanoic acid (1R,2R,3S,4S,5R,6S)-2,3,4,5-tetrakis-benzyloxy-6-[benzyloxy-((R)-2-hexadecanoyloxy-3-hexanoyloxy-propoxy)-phosphoryloxy]-cyclohexyl ester

Guidance literature:: Multi-step reaction with 6 steps

1.1: dibutyltin oxide / 3 h

1.2: 96 percent / cesium fluoride / toluene; dimethylformamide / -10 - 20 °C

2.1: 99 percent / pyridine / 0 - 20 °C

3.1: 35 percent / PdCl₂; NaOAc / acetic acid; H₂O / 20 °C

4.1: 82 percent / N,N-diisopropylammonium tetrazolide / CH₂Cl₂ / 5 h / 20 °C

5.1: 1H-tetrazole / CH₂Cl₂ / Heating

6.1: m-chloroperoxybenzoic acid / CH₂Cl₂ / -40 - 20 °C

With 1H-tetrazole; N,N-diisopropylamine tetrazolide; sodium acetate; di(n-butyl)tin oxide; 3-chloro-benzenecarboperoxoic acid; palladium dichloride; In pyridine; dichloromethane; water; acetic acid;
DOI:10.1021/ol0202161