C₁₂H₁₀ClN₃O₂

Base Information

Chemical Name:C₁₂H₁₀ClN₃O₂
CAS No.:1333153-35-7
Molecular Formula:C₁₂H₁₀ClN₃O₂
Molecular Weight:263.683
Hs Code.:

C<sub>12</sub>H<sub>10</sub>ClN<sub>3</sub>O<sub>2</sub>

Synonyms:C₁₂H₁₀ClN₃O₂

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Chemical Property of C₁₂H₁₀ClN₃O₂

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Technology Process of C₁₂H₁₀ClN₃O₂

There total 5 articles about C₁₂H₁₀ClN₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1333153-34-6
C₁₄H₁₄ClN₃O₂

: 1333153-35-7
C₁₂H₁₀ClN₃O₂

Guidance literature:: C₁₄H₁₄ClN₃O₂; With water; lithium hydroxide; In tetrahydrofuran; at 20 ℃; for 0.75h;

With hydrogenchloride; In tetrahydrofuran; water; pH=2;

Reference yield:

: 766-84-7
3-chloro-benzonitrile

: 1333153-35-7
C₁₂H₁₀ClN₃O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: magnesium(II) chloride hexahydrate; sodium monohydrogen sulfide x-hydrate / N,N-dimethyl-formamide / 2 h / 20 °C

2.1: diethyl ether / 24 h

3.1: N,N-dimethyl-formamide / 90 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

4.2: 0 - 80 °C

5.1: water; lithium hydroxide / tetrahydrofuran / 0.75 h / 20 °C

5.2: pH 2

With sodium monohydrogen sulfide x-hydrate; magnesium(II) chloride hexahydrate; water; sodium hydride; lithium hydroxide; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;

Reference yield:

: 2548-79-0
3-chlorothiobenzamide

: 1333153-35-7
C₁₂H₁₀ClN₃O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: diethyl ether / 24 h

2.1: N,N-dimethyl-formamide / 90 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

3.2: 0 - 80 °C

4.1: water; lithium hydroxide / tetrahydrofuran / 0.75 h / 20 °C

4.2: pH 2

With water; sodium hydride; lithium hydroxide; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;