alpha-D-glucopyranoside,methyl,3-benzoate 2,6-bis(4-methylbenzenesulfonate)

Base Information

Chemical Name:alpha-D-glucopyranoside,methyl,3-benzoate 2,6-bis(4-methylbenzenesulfonate)
CAS No.:165375-09-7
Molecular Formula:C28H30 O11 S2
Molecular Weight:606.66
Hs Code.:
Mol file:165375-09-7.mol

Synonyms:.Alpha.-D-glucopyranoside,methyl,3-benzoate 2,6-bis(4-methylbenzenesulfonate);165375-09-7

Suppliers and Price of alpha-D-glucopyranoside,methyl,3-benzoate 2,6-bis(4-methylbenzenesulfonate)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of alpha-D-glucopyranoside,methyl,3-benzoate 2,6-bis(4-methylbenzenesulfonate)

Chemical Property:

Boiling Point:765.4±60.0 °C(Predicted)
PKA:12.12±0.70(Predicted)
PSA：168.49000
Density:1.45±0.1 g/cm3(Predicted)
LogP:4.90220
XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:11
Rotatable Bond Count:11
Exact Mass:606.12295412
Heavy Atom Count:41
Complexity:1050

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)OCC2C(C(C(C(O2)OC)OS(=O)(=O)C3=CC=C(C=C3)C)OC(=O)C4=CC=CC=C4)O
Isomeric SMILES:CC1=CC=C(C=C1)S(=O)(=O)OC[C@@H]2[C@H]([C@@H]([C@H]([C@H](O2)OC)OS(=O)(=O)C3=CC=C(C=C3)C)OC(=O)C4=CC=CC=C4)O

Technology Process of alpha-D-glucopyranoside,methyl,3-benzoate 2,6-bis(4-methylbenzenesulfonate)

There total 1 articles about alpha-D-glucopyranoside,methyl,3-benzoate 2,6-bis(4-methylbenzenesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 54497-89-1
methyl 2,6-bis-α-D-glucopyranoside

: 98-88-4
benzoyl chloride

: 96711-93-2
methyl 3,4-di-O-benzoyl-2,6-di-O-tosyl-α-D-glucopyranoside

: 165375-09-7
methyl 3-O-benzoyl-2,6-di-O-tosyl-α-D-glucopyranoside

Guidance literature:: In pyridine; 1.) 0 deg C, 7 h, 2.) 20 deg C, 30 h;

Reference yield: 86.0%

: 108-24-7
acetic anhydride

: 165375-09-7
methyl 3-O-benzoyl-2,6-di-O-tosyl-α-D-glucopyranoside

: 165375-10-0
methyl 4-O-acetyl-3-O-benzoyl-2,6-di-O-tosyl-α-D-glucopyranoside

Guidance literature:: In pyridine; at 20 ℃; for 1h;

Reference yield:

: 165375-09-7
methyl 3-O-benzoyl-2,6-di-O-tosyl-α-D-glucopyranoside

: 165375-15-5
Benzoic acid (1R,4R,5R)-5-acetoxy-4-hydroxymethyl-cyclopent-2-enyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 86 percent / pyridine / 1 h / 20 °C

2: 83 percent / NaI / acetic anhydride / 1 h / Heating

3: Zn / ethanol / Heating

4: 57 percent / ethanol; pyridine / 1.6 h / 45 °C

5: 68 percent / H₂ / Raney nickel

6: 81 percent / magnesium monoperoxyphthalate hexahydrate / propan-2-ol

With hydrogen; magnesium monoperoxyphthalate hexahydrate; sodium iodide; zinc; nickel; In pyridine; ethanol; acetic anhydride; isopropyl alcohol;