N-methyl-N-pyridin-2-ylmethyl-N'-(2,4,6-trimethyl-phenyl)-ethane-1,2-diamine

Base Information

Chemical Name:N-methyl-N-pyridin-2-ylmethyl-N'-(2,4,6-trimethyl-phenyl)-ethane-1,2-diamine
CAS No.:863986-80-5
Molecular Formula:C₁₈H₂₅N₃
Molecular Weight:283.417
Hs Code.:

<i>N</i>-methyl-<i>N</i>-pyridin-2-ylmethyl-<i>N</i>'-(2,4,6-trimethyl-phenyl)-ethane-1,2-diamine

Synonyms:N-methyl-N-pyridin-2-ylmethyl-N'-(2,4,6-trimethyl-phenyl)-ethane-1,2-diamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-N-pyridin-2-ylmethyl-N'-(2,4,6-trimethyl-phenyl)-ethane-1,2-diamine

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Technology Process of N-methyl-N-pyridin-2-ylmethyl-N'-(2,4,6-trimethyl-phenyl)-ethane-1,2-diamine

There total 1 articles about N-methyl-N-pyridin-2-ylmethyl-N'-(2,4,6-trimethyl-phenyl)-ethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 74-88-4
methyl iodide

: 769193-60-4
((2,4,6-Me₃C₆H₂)HNCH₂CH₂)((2-C₅H₄N)CH₂)NH

: 863986-80-5
N-methyl-N-pyridin-2-ylmethyl-N'-(2,4,6-trimethyl-phenyl)-ethane-1,2-diamine

: dimethyl-pyridin-2-ylmethyl-[2-(2,4,6-trimethyl-phenylamino)-ethyl]-ammonium; iodide

Guidance literature:: With potassium carbonate; In acetonitrile; at -10 - 20 ℃;
DOI:10.1039/b505763a

Reference yield: 72.0%

: 863986-80-5
N-methyl-N-pyridin-2-ylmethyl-N'-(2,4,6-trimethyl-phenyl)-ethane-1,2-diamine

: cobalt(II) chloride hexahydrate

: CoCl₂(NC₅H₄CH₂N(CH₃)CH₂CH₂NHC₆H₂(CH₃)3)

Guidance literature:: In tetrahydrofuran; under N2; ligand (1 equiv.) added to Co salt in THF at room temp.; stirred at room temp. for 24 h; concd.; hexane added; stirred overnight; filtered; ppt. washed with hexane; dried under reduced pressure; elem. anal.;
DOI:10.1039/b505763a

Reference yield: 66.0%

: 863986-80-5
N-methyl-N-pyridin-2-ylmethyl-N'-(2,4,6-trimethyl-phenyl)-ethane-1,2-diamine

: iron(II) chloride*1.5THF

: 863986-74-7
FeCl₂(NC₅H₄CH₂N(CH₃)CH₂CH₂NHC₆H₂(CH₃)3)

Guidance literature:: In tetrahydrofuran; under N2; ligand (1 equiv.) added to Fe complex in THF at room temp.; stirred at room temp. for 24 h; concd.; hexane added; stirred overnight; filtered; ppt. washed with hexane; dried under reduced pressure; elem. anal.;
DOI:10.1039/b505763a