(5-cyano-2-(2,2,2-trifluoroacetamido)benzyl)triphenylphosphonium chloride

Base Information

Chemical Name:(5-cyano-2-(2,2,2-trifluoroacetamido)benzyl)triphenylphosphonium chloride
CAS No.:1192152-63-8
Molecular Formula:C₂₈H₂₁F₃N₂OP*Cl
Molecular Weight:524.91
Hs Code.:

Synonyms:(5-cyano-2-(2,2,2-trifluoroacetamido)benzyl)triphenylphosphonium chloride

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Chemical Property of (5-cyano-2-(2,2,2-trifluoroacetamido)benzyl)triphenylphosphonium chloride

Chemical Property:

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Technology Process of (5-cyano-2-(2,2,2-trifluoroacetamido)benzyl)triphenylphosphonium chloride

There total 3 articles about (5-cyano-2-(2,2,2-trifluoroacetamido)benzyl)triphenylphosphonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1192152-64-9
N-(2-(chloromethyl)-4-cyanophenyl)-2,2,2-trifluoroacetamide

: 603-35-0
triphenylphosphine

: 1192152-63-8
(5-cyano-2-(2,2,2-trifluoroacetamido)benzyl)triphenylphosphonium chloride

Guidance literature:: In toluene; at 100 ℃; for 6h; Inert atmosphere;

Reference yield:

: 78881-21-7
4-amino-3-methylbenzonitrile

: 1192152-63-8
(5-cyano-2-(2,2,2-trifluoroacetamido)benzyl)triphenylphosphonium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 0 - 20 °C

2: dibenzoyl peroxide; sulfuryl dichloride / tetrachloromethane / 3 h / 100 °C

3: toluene / 3 h / 110 °C

With sulfuryl dichloride; triethylamine; dibenzoyl peroxide; In tetrachloromethane; dichloromethane; toluene;

Reference yield:

: 943634-40-0
N-(4-cyano-2-methylphenyl)-2,2,2-trifluoroacetamide

: 1192152-63-8
(5-cyano-2-(2,2,2-trifluoroacetamido)benzyl)triphenylphosphonium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: dibenzoyl peroxide; sulfuryl dichloride / tetrachloromethane / 3 h / 100 °C

2: toluene / 3 h / 110 °C

With sulfuryl dichloride; dibenzoyl peroxide; In tetrachloromethane; toluene;