Technology Process of meso-2,3-diveratryl-succinic acid dimethyl ester
There total 13 articles about meso-2,3-diveratryl-succinic acid dimethyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 67 percent / trifluoroacetic anhydride / 3 h / Heating
2: 86 percent / H2 / 10percent Pd/C / ethyl acetate / 32 h / 3102.9 Torr
3: 78 percent / H2SO4 / toluene / 32 h / Heating
4: 92 percent / H2 / 10percent Pd/C / ethyl acetate / 18 h / 3102.9 Torr
With
sulfuric acid; hydrogen; trifluoroacetic anhydride;
palladium on activated charcoal;
In
ethyl acetate; toluene;
DOI:10.1016/0040-4020(96)00761-2
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 98 percent / potassium t-butoxide / 2-methyl-propan-2-ol / 3 h / Heating
2: 79 percent / H2SO4 / toluene / 16 h / Heating
3: 48 percent / potassium t-butoxide / 2-methyl-propan-2-ol / 3 h / Heating
4: 82 percent / 1.) 2M aq. NaOH, 2.) aq. HCl / 12 h / Heating
5: 67 percent / trifluoroacetic anhydride / 3 h / Heating
6: 86 percent / H2 / 10percent Pd/C / ethyl acetate / 32 h / 3102.9 Torr
7: 78 percent / H2SO4 / toluene / 32 h / Heating
8: 92 percent / H2 / 10percent Pd/C / ethyl acetate / 18 h / 3102.9 Torr
With
hydrogenchloride; sodium hydroxide; sulfuric acid; potassium tert-butylate; hydrogen; trifluoroacetic anhydride;
palladium on activated charcoal;
In
ethyl acetate; toluene; tert-butyl alcohol;
DOI:10.1016/0040-4020(96)00761-2
