1-(4-methoxyphenyl)-1H-[1,2,4]triazol-4-ium-4-methoxybenzoyl-2,4,6-trinitrophenylmethylide

Base Information

Chemical Name:1-(4-methoxyphenyl)-1H-[1,2,4]triazol-4-ium-4-methoxybenzoyl-2,4,6-trinitrophenylmethylide
CAS No.:263152-07-4
Molecular Formula:C₂₄H₁₈N₆O₉
Molecular Weight:534.442
Hs Code.:

Synonyms:1-(4-methoxyphenyl)-1H-[1,2,4]triazol-4-ium-4-methoxybenzoyl-2,4,6-trinitrophenylmethylide

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Chemical Property of 1-(4-methoxyphenyl)-1H-[1,2,4]triazol-4-ium-4-methoxybenzoyl-2,4,6-trinitrophenylmethylide

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Technology Process of 1-(4-methoxyphenyl)-1H-[1,2,4]triazol-4-ium-4-methoxybenzoyl-2,4,6-trinitrophenylmethylide

There total 4 articles about 1-(4-methoxyphenyl)-1H-[1,2,4]triazol-4-ium-4-methoxybenzoyl-2,4,6-trinitrophenylmethylide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 88-88-0
2,4,6-trinitrochlorobenzene

: 1-(4-methoxyphenyl)-4-(4-methoxy)phenacyl-1H-[1,2,4]triazol-4-ium bromide

: 263152-07-4
1-(4-methoxyphenyl)-1H-[1,2,4]triazol-4-ium-4-methoxybenzoyl-2,4,6-trinitrophenylmethylide

Guidance literature:: With triethylamine; In chloroform; at 0 - 20 ℃; for 3h;
DOI:10.1016/S0040-4020(99)01006-6

Reference yield:

: 68377-33-3
1-(4-methoxyphenyl)-1H-[1,2,4]triazole

: 263152-07-4
1-(4-methoxyphenyl)-1H-[1,2,4]triazol-4-ium-4-methoxybenzoyl-2,4,6-trinitrophenylmethylide

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / acetone / 8 h / Heating

2: 75 percent / Et₃N / CHCl₃ / 3 h / 0 - 20 °C

With triethylamine; In chloroform; acetone; 1: Addition / 2: Arylation;
DOI:10.1016/S0040-4020(99)01006-6

Reference yield:

: 68337-15-5
4-(1,2,4-triazol-1-yl)phenol

: 263152-07-4
1-(4-methoxyphenyl)-1H-[1,2,4]triazol-4-ium-4-methoxybenzoyl-2,4,6-trinitrophenylmethylide

Guidance literature:: Multi-step reaction with 3 steps

1: KOH / ethanol / 12 h / Heating

2: 65 percent / acetone / 8 h / Heating

3: 75 percent / Et₃N / CHCl₃ / 3 h / 0 - 20 °C

With potassium hydroxide; triethylamine; In ethanol; chloroform; acetone; 1: Methylation / 2: Addition / 3: Arylation;
DOI:10.1016/S0040-4020(99)01006-6