monobenzyl 3-methylglutarate

Base Information

Chemical Name:monobenzyl 3-methylglutarate
CAS No.:13853-23-1
Molecular Formula:C₁₃H₁₆O₄
Molecular Weight:236.268
Hs Code.:

Synonyms:monobenzyl 3-methylglutarate

Suppliers and Price of monobenzyl 3-methylglutarate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of monobenzyl 3-methylglutarate

Chemical Property:

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Technology Process of monobenzyl 3-methylglutarate

There total 4 articles about monobenzyl 3-methylglutarate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 3-methyl-pentanedioic acid benzyl ester naphthalen-2-ylmethyl ester

: 13853-23-1
monobenzyl 3-methylglutarate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; ethyl acetate; for 1.33333h; under 760 Torr;
DOI:10.1016/S0040-4039(99)00014-3

Reference yield: 43.0%

: 4166-53-4
3-methylglutaric anhydride

: 100-51-6,185532-71-2
benzyl alcohol

: 13853-23-1
monobenzyl 3-methylglutarate

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 72h;

Reference yield:

: 1668-10-6
glycinamide hydrochloride

: 341926-05-4
dibenzyl 3-methylglutarate

: 13853-23-1
monobenzyl 3-methylglutarate

: (R)-4-(Carbamoylmethyl-carbamoyl)-3-methyl-butyric acid benzyl ester

: monobenzyl 3-methylglutaryl-Gly-NH₂

Guidance literature:: With subtilisin bacillus lentus S₁₆₆C-S-CH₂C₆F₅ mutant enzyme; triethylamine; In water; N,N-dimethyl-formamide; at 20 ℃; for 120h; Title compound not separated from byproducts;
DOI:10.1016/S0957-4166(01)00024-6