4-{2-[2-(2-Methyl-[1,3]dioxolan-2-ylmethyl)-[1,3]dioxolan-2-yl]-ethyl}-phenylamine

Base Information

Chemical Name:4-{2-[2-(2-Methyl-[1,3]dioxolan-2-ylmethyl)-[1,3]dioxolan-2-yl]-ethyl}-phenylamine
CAS No.:782475-32-5
Molecular Formula:C₁₆H₂₃NO₄
Molecular Weight:293.363
Hs Code.:

Synonyms:4-{2-[2-(2-Methyl-[1,3]dioxolan-2-ylmethyl)-[1,3]dioxolan-2-yl]-ethyl}-phenylamine

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Chemical Property of 4-{2-[2-(2-Methyl-[1,3]dioxolan-2-ylmethyl)-[1,3]dioxolan-2-yl]-ethyl}-phenylamine

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Technology Process of 4-{2-[2-(2-Methyl-[1,3]dioxolan-2-ylmethyl)-[1,3]dioxolan-2-yl]-ethyl}-phenylamine

There total 4 articles about 4-{2-[2-(2-Methyl-[1,3]dioxolan-2-ylmethyl)-[1,3]dioxolan-2-yl]-ethyl}-phenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 782475-33-6
C₁₆H₂₁NO₆

: 782475-32-5
4-{2-[2-(2-Methyl-[1,3]dioxolan-2-ylmethyl)-[1,3]dioxolan-2-yl]-ethyl}-phenylamine

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 2h; under 2585.81 Torr; Parr shaker;

Reference yield:

: 192650-25-2
6-(4-nitrophenyl)hexane-2,4-dione

: 782475-32-5
4-{2-[2-(2-Methyl-[1,3]dioxolan-2-ylmethyl)-[1,3]dioxolan-2-yl]-ethyl}-phenylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / pTSA / toluene / Heating

2: 95 percent / H₂ / Pd/C / ethyl acetate

With hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In ethyl acetate; toluene;
DOI:10.1016/j.bmcl.2006.10.009

Reference yield:

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 782475-32-5
4-{2-[2-(2-Methyl-[1,3]dioxolan-2-ylmethyl)-[1,3]dioxolan-2-yl]-ethyl}-phenylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 40 percent / LDA / hexamethylphosphoric acid triamide / -78 °C

2: 65 percent / pTSA / toluene / Heating

3: 95 percent / H₂ / Pd/C / ethyl acetate

With hydrogen; toluene-4-sulfonic acid; lithium diisopropyl amide; palladium on activated charcoal; In N,N,N,N,N,N-hexamethylphosphoric triamide; ethyl acetate; toluene;
DOI:10.1016/j.bmcl.2006.10.009