(1S,3S,5R,6R,8R)-5-<(1R)-1,2-dihydroxyethyl>-3,8-diphenyl-2,4,7,9-tetraoxabicyclo<4.4.0>decane

Base Information

Chemical Name:(1S,3S,5R,6R,8R)-5-<(1R)-1,2-dihydroxyethyl>-3,8-diphenyl-2,4,7,9-tetraoxabicyclo<4.4.0>decane
CAS No.:61473-59-4
Molecular Formula:C₂₀H₂₂O₆
Molecular Weight:358.391
Hs Code.:

Synonyms:(1S,3S,5R,6R,8R)-5-<(1R)-1,2-dihydroxyethyl>-3,8-diphenyl-2,4,7,9-tetraoxabicyclo<4.4.0>decane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,3S,5R,6R,8R)-5-<(1R)-1,2-dihydroxyethyl>-3,8-diphenyl-2,4,7,9-tetraoxabicyclo<4.4.0>decane

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Technology Process of (1S,3S,5R,6R,8R)-5-<(1R)-1,2-dihydroxyethyl>-3,8-diphenyl-2,4,7,9-tetraoxabicyclo<4.4.0>decane

There total 5 articles about (1S,3S,5R,6R,8R)-5-<(1R)-1,2-dihydroxyethyl>-3,8-diphenyl-2,4,7,9-tetraoxabicyclo<4.4.0>decane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 4148-67-8
1,3:2,4:5,6-tri-O-benzylidene-D-glucitol

: 19046-64-1,19046-65-2,61473-59-4,78512-85-3,112923-92-9,121252-47-9,32647-67-9
1,3:2,4-di-O-benzylidene-D-glucitol

Guidance literature:: With ammonium formate; palladium on activated charcoal; In methanol; for 0.666667h; Heating;
DOI:10.1016/0008-6215(85)85137-5

Reference yield: 60.0%

: 50-70-4
D-sorbitol

: 100-52-7
benzaldehyde

: 61473-59-4
(1S,3S,5R,6R,8R)-5-<(1R)-1,2-dihydroxyethyl>-3,8-diphenyl-2,4,7,9-tetraoxabicyclo<4.4.0>decane

Guidance literature:: With toluene-4-sulfonic acid; In cyclohexane; at 80 ℃;
DOI:10.1246/bcsj.71.1457

Reference yield:

: 50-70-4
D-sorbitol

: 100-52-7
benzaldehyde

: 19046-64-1,19046-65-2,61473-59-4,78512-85-3,112923-92-9,121252-47-9,32647-67-9
1,3:2,4-di-O-benzylidene-D-glucitol

Guidance literature:: With hydrogenchloride; at 20 ℃; Umsetzen des Reaktionsprodukts mit Benzoylchlorid in Pyridin und Behandeln einer Chloroform-Loesung des Reaktionsprodukts mit kalter Natriummethylat-Loesung;