C₂₇H₃₆BrNO₂

Base Information

Chemical Name:C₂₇H₃₆BrNO₂
CAS No.:1448022-65-8
Molecular Formula:C₂₇H₃₆BrNO₂
Molecular Weight:486.492
Hs Code.:

C<sub>27</sub>H<sub>36</sub>BrNO<sub>2</sub>

Synonyms:C₂₇H₃₆BrNO₂

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Chemical Property of C₂₇H₃₆BrNO₂

Chemical Property:

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Technology Process of C₂₇H₃₆BrNO₂

There total 3 articles about C₂₇H₃₆BrNO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 70614-87-8
6α,7α-epoxy-12-methoxyferruginol

: 106-40-1
4-bromo-aniline

: 1448022-65-8
C₂₇H₃₆BrNO₂

Guidance literature:: With zinc dibromide; In acetonitrile; for 15h; Reflux;
DOI:10.1016/j.tetlet.2013.06.048

Reference yield:

: 79593-19-4
(+)-(4aS,10aS)-6-acetyl-7-isopropyl-1,1,4a-trimethyl-1,2,3,4,4a,9,10,10a-octahydrophenanthrene

: 1448022-65-8
C₂₇H₃₆BrNO₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: 3-chloro-benzenecarboperoxoic acid; toluene-4-sulfonic acid / 1,2-dichloro-ethane / 5 h / Reflux

2.1: potassium carbonate / dichloromethane; methanol / 2 h / 0 °C

3.1: lithium hydroxide / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere

3.2: 0.75 h / 0 °C

4.1: chromium(VI) oxide; acetic acid / 4 h / 20 °C

5.1: sodium tetrahydroborate / methanol / 12 h / 20 °C / Inert atmosphere

6.1: methanesulfonyl chloride; triethylamine / dichloromethane / 12 h / 0 °C / Inert atmosphere

7.1: 3,3-dimethyldioxirane / dichloromethane; acetone / 1 h / -25 °C

8.1: zinc dibromide / acetonitrile / 15 h / Reflux

With chromium(VI) oxide; sodium tetrahydroborate; 3,3-dimethyldioxirane; potassium carbonate; toluene-4-sulfonic acid; acetic acid; methanesulfonyl chloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; zinc dibromide; lithium hydroxide; In methanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; acetonitrile; 1.1: |Baeyer-Villiger Ketone Oxidation;
DOI:10.1016/j.tetlet.2013.06.048

Reference yield:

: 19407-28-4
ar-abietatriene

: 1448022-65-8
C₂₇H₃₆BrNO₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: aluminum (III) chloride / dichloromethane / 24 h / 20 °C / Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid; toluene-4-sulfonic acid / 1,2-dichloro-ethane / 5 h / Reflux

3.1: potassium carbonate / dichloromethane; methanol / 2 h / 0 °C

4.1: lithium hydroxide / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere

4.2: 0.75 h / 0 °C

5.1: chromium(VI) oxide; acetic acid / 4 h / 20 °C

6.1: sodium tetrahydroborate / methanol / 12 h / 20 °C / Inert atmosphere

7.1: methanesulfonyl chloride; triethylamine / dichloromethane / 12 h / 0 °C / Inert atmosphere

8.1: 3,3-dimethyldioxirane / dichloromethane; acetone / 1 h / -25 °C

9.1: zinc dibromide / acetonitrile / 15 h / Reflux

With chromium(VI) oxide; aluminum (III) chloride; sodium tetrahydroborate; 3,3-dimethyldioxirane; potassium carbonate; toluene-4-sulfonic acid; acetic acid; methanesulfonyl chloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; zinc dibromide; lithium hydroxide; In methanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; acetonitrile; 2.1: |Baeyer-Villiger Ketone Oxidation;
DOI:10.1016/j.tetlet.2013.06.048