1,2-dihydroperfluorocyclohexanol

Base Information

Chemical Name:1,2-dihydroperfluorocyclohexanol
CAS No.:83505-07-1
Molecular Formula:C₆H₃F₉O
Molecular Weight:262.075
Hs Code.:

Synonyms:1,2-dihydroperfluorocyclohexanol

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Chemical Property of 1,2-dihydroperfluorocyclohexanol

Chemical Property:

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Technology Process of 1,2-dihydroperfluorocyclohexanol

There total 2 articles about 1,2-dihydroperfluorocyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.4%

: 5927-67-3
decafluoro-1,2-epoxycyclohexane

: 83505-07-1
1,2-dihydroperfluorocyclohexanol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 1h;

Reference yield:

: 355-75-9
decafluorocyclohex-1-ene

: 83505-07-1
1,2-dihydroperfluorocyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / sodium hypochlorite / H₂O; acetonitrile / 1 h

2: 72.4 percent / lithium aluminum hydride / diethyl ether / 1 h

With sodium hypochlorite; lithium aluminium tetrahydride; In diethyl ether; water; acetonitrile;

Reference yield:

: 83505-07-1
1,2-dihydroperfluorocyclohexanol

: 2H-octafluorocyclohex-1-ene-1-yl methoxymethyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium hydride / 1.) benzene, 30 min, 15 deg C; 2.) 1 h

2: 4.1 g / 6 M potassium hydoxide, silicone antifoaming agent / 2 h / Heating

With silicone antifoaming agent; potassium hydroxide; sodium hydride;
DOI:10.1016/S0022-1139(00)82291-5