N-(N-4-propionamidobenzoyl-L-phenylalanyl)-L-phenylalanine methyl ester

Base Information

Chemical Name:N-(N-4-propionamidobenzoyl-L-phenylalanyl)-L-phenylalanine methyl ester
CAS No.:934221-25-7
Molecular Formula:C₂₉H₃₁N₃O₅
Molecular Weight:501.582
Hs Code.:

Synonyms:N-(N-4-propionamidobenzoyl-L-phenylalanyl)-L-phenylalanine methyl ester

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Chemical Property of N-(N-4-propionamidobenzoyl-L-phenylalanyl)-L-phenylalanine methyl ester

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Technology Process of N-(N-4-propionamidobenzoyl-L-phenylalanyl)-L-phenylalanine methyl ester

There total 5 articles about N-(N-4-propionamidobenzoyl-L-phenylalanyl)-L-phenylalanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₂₀N₂O₄

: 7524-50-7
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

: 934221-25-7
N-(N-4-propionamidobenzoyl-L-phenylalanyl)-L-phenylalanine methyl ester

Guidance literature:: With 4-methyl-morpholine; isobutyl chloroformate; In dichloromethane; at 0 ℃; for 1.5h;
DOI:10.1016/j.bmc.2011.08.001

Reference yield:

: 19313-85-0
4-propionamidobenzoic acid

: 934221-25-7
N-(N-4-propionamidobenzoyl-L-phenylalanyl)-L-phenylalanine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 4-methyl-morpholine; isobutyl chloroformate / dichloromethane / 1.5 h / 0 °C

2.1: sodium hydroxide / N,N-dimethyl-formamide / 2 h / 20 °C

2.2: 20 °C / pH 6 - 7

3.1: 4-methyl-morpholine; isobutyl chloroformate / dichloromethane / 1.5 h / 0 °C

With 4-methyl-morpholine; sodium hydroxide; isobutyl chloroformate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.08.001

Reference yield:

: C₂₀H₂₂N₂O₄

: 934221-25-7
N-(N-4-propionamidobenzoyl-L-phenylalanyl)-L-phenylalanine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / N,N-dimethyl-formamide / 2 h / 20 °C

1.2: 20 °C / pH 6 - 7

2.1: 4-methyl-morpholine; isobutyl chloroformate / dichloromethane / 1.5 h / 0 °C

With 4-methyl-morpholine; sodium hydroxide; isobutyl chloroformate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.08.001