ethyl 3-oxo-3-ethyl-N-benzyl>aminopropionate

Base Information

Chemical Name:ethyl 3-oxo-3-ethyl-N-benzyl>aminopropionate
CAS No.:154308-12-0
Molecular Formula:C₂₆H₂₈N₂O₅
Molecular Weight:448.519
Hs Code.:

ethyl 3-oxo-3-<N-<2-ethoxycarbonyl-1-(2-quinolinyl)>ethyl-N-benzyl>aminopropionate

Synonyms:ethyl 3-oxo-3-ethyl-N-benzyl>aminopropionate

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Chemical Property of ethyl 3-oxo-3-ethyl-N-benzyl>aminopropionate

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Technology Process of ethyl 3-oxo-3-ethyl-N-benzyl>aminopropionate

There total 4 articles about ethyl 3-oxo-3-ethyl-N-benzyl>aminopropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1071-46-1
hydrogen ethyl malonate

: 154308-08-4
ethyl 3-benzylamino-3-(2-quinolinyl)propionate

: 154308-12-0
ethyl 3-oxo-3-ethyl-N-benzyl>aminopropionate

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; for 0.5h; Ambient temperature;
DOI:10.1002/jhet.5570300311

Reference yield:

: 96057-59-9
ethyl 3-oxo-3-(quinolin-2-yl)propanoate

: 154308-12-0
ethyl 3-oxo-3-ethyl-N-benzyl>aminopropionate

Guidance literature:: Multi-step reaction with 3 steps

1: formic acid / benzene / Heating

2: H₂, NaBH₄ / 10percent Pd/C / methanol / 18 h / 735.5 Torr

3: 79 percent / dicyclohexylcarbodiimide (DCC) / CH₂Cl₂ / 0.5 h / Ambient temperature

With sodium tetrahydroborate; formic acid; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane; benzene;
DOI:10.1002/jhet.5570300311

Reference yield:

: 3-[(Z)-Benzylimino]-3-quinolin-2-yl-propionic acid ethyl ester

: 154308-12-0
ethyl 3-oxo-3-ethyl-N-benzyl>aminopropionate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂, NaBH₄ / 10percent Pd/C / methanol / 18 h / 735.5 Torr

2: 79 percent / dicyclohexylcarbodiimide (DCC) / CH₂Cl₂ / 0.5 h / Ambient temperature

With sodium tetrahydroborate; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1002/jhet.5570300311