(E)-4,4'-Bis-(3-azido-propylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene]

Base Information

• Chemical Name: (E)-4,4'-Bis-(3-azido-propylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene]
• CAS No.: 127691-89-8
• Molecular Formula: C₂₄H₂₀Cl₂N₆S₆
• Molecular Weight: 655.765

Synonyms:(E)-4,4'-Bis-(3-azido-propylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene]

Chemical Property of (E)-4,4'-Bis-(3-azido-propylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene]

Chemical Property:

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Technology Process of (E)-4,4'-Bis-(3-azido-propylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene]

There total 2 articles about (E)-4,4'-Bis-(3-azido-propylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

(E)-4,4'-Bis-(3-bromo-propylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene] (127679-38-3) → (E)-4,4'-Bis-(3-azido-propylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene] (127691-89-8)

Guidance literature:

With sodium azide; In dimethyl sulfoxide; at 60 ℃;

DOI:10.1016/S0040-4020(01)85427-2

Reference yield:

4-(3-Bromo-propylsulfanyl)-5-(4-chloro-phenyl)-2-ethoxy-[1,3]dithiole (127679-48-5) → (E)-4,4'-Bis-(3-azido-propylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene] (127691-89-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / trichloroacetic acid / benzene / 1 h / Heating

2: 87 percent / NaN₃ / dimethylsulfoxide / 60 °C

With sodium azide; trichloroacetic acid; In dimethyl sulfoxide; benzene;

DOI:10.1016/S0040-4020(01)85427-2

Reference yield: 100.0%

(E)-4,4'-Bis-(3-azido-propylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene] (127691-89-8) → (3-{(E)-5,5'-Bis-(4-chloro-phenyl)-4'-[3-(dimethoxy-phosphorylamino)-propylsulfanyl]-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl}-propyl)-phosphoramidic acid dimethyl ester (127679-55-4)

Guidance literature:

With phosphorous acid trimethyl ester; In tetrahydrofuran; water; at 45 ℃;

DOI:10.1016/S0040-4020(01)85427-2

upstream raw materials:

(E)-4,4'-Bis-(3-bromo-propylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene]

4-(3-Bromo-propylsulfanyl)-5-(4-chloro-phenyl)-2-ethoxy-[1,3]dithiole

Downstream raw materials:

(3-{(E)-5,5'-Bis-(4-chloro-phenyl)-4'-[3-(dimethoxy-phosphorylamino)-propylsulfanyl]-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl}-propyl)-phosphoramidic acid dimethyl ester

3-[(E)-4'-(3-Amino-propylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl]-propylamine

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