(3-{(E)-5,5'-Bis-(4-chloro-phenyl)-4'-[3-(dimethoxy-phosphorylamino)-propylsulfanyl]-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl}-propyl)-phosphoramidic acid dimethyl ester

Base Information

Chemical Name:(3-{(E)-5,5'-Bis-(4-chloro-phenyl)-4'-[3-(dimethoxy-phosphorylamino)-propylsulfanyl]-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl}-propyl)-phosphoramidic acid dimethyl ester
CAS No.:127679-55-4
Molecular Formula:C₂₈H₃₄Cl₂N₂O₆P₂S₆
Molecular Weight:819.837
Hs Code.:

(3-{(E)-5,5'-Bis-(4-chloro-phenyl)-4'-[3-(dimethoxy-phosphorylamino)-propylsulfanyl]-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl}-propyl)-phosphoramidic acid dimethyl ester

Synonyms:(3-{(E)-5,5'-Bis-(4-chloro-phenyl)-4'-[3-(dimethoxy-phosphorylamino)-propylsulfanyl]-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl}-propyl)-phosphoramidic acid dimethyl ester

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Chemical Property of (3-{(E)-5,5'-Bis-(4-chloro-phenyl)-4'-[3-(dimethoxy-phosphorylamino)-propylsulfanyl]-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl}-propyl)-phosphoramidic acid dimethyl ester

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Technology Process of (3-{(E)-5,5'-Bis-(4-chloro-phenyl)-4'-[3-(dimethoxy-phosphorylamino)-propylsulfanyl]-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl}-propyl)-phosphoramidic acid dimethyl ester

There total 3 articles about (3-{(E)-5,5'-Bis-(4-chloro-phenyl)-4'-[3-(dimethoxy-phosphorylamino)-propylsulfanyl]-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl}-propyl)-phosphoramidic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 127691-89-8
(E)-4,4'-Bis-(3-azido-propylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene]

: 127679-55-4
(3-{(E)-5,5'-Bis-(4-chloro-phenyl)-4'-[3-(dimethoxy-phosphorylamino)-propylsulfanyl]-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl}-propyl)-phosphoramidic acid dimethyl ester

Guidance literature:: With phosphorous acid trimethyl ester; In tetrahydrofuran; water; at 45 ℃;
DOI:10.1016/S0040-4020(01)85427-2

Reference yield:

: 127679-48-5
4-(3-Bromo-propylsulfanyl)-5-(4-chloro-phenyl)-2-ethoxy-[1,3]dithiole

: 127679-55-4
(3-{(E)-5,5'-Bis-(4-chloro-phenyl)-4'-[3-(dimethoxy-phosphorylamino)-propylsulfanyl]-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl}-propyl)-phosphoramidic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / trichloroacetic acid / benzene / 1 h / Heating

2: 87 percent / NaN₃ / dimethylsulfoxide / 60 °C

3: 100 percent / P(OMe)3 / tetrahydrofuran; H₂O / 45 °C

With sodium azide; phosphorous acid trimethyl ester; trichloroacetic acid; In tetrahydrofuran; water; dimethyl sulfoxide; benzene;
DOI:10.1016/S0040-4020(01)85427-2

Reference yield:

: 127679-38-3
(E)-4,4'-Bis-(3-bromo-propylsulfanyl)-5,5'-bis-(4-chloro-phenyl)-[2,2']bi[[1,3]dithiolylidene]

: 127679-55-4
(3-{(E)-5,5'-Bis-(4-chloro-phenyl)-4'-[3-(dimethoxy-phosphorylamino)-propylsulfanyl]-[2,2']bi[[1,3]dithiolylidene]-4-ylsulfanyl}-propyl)-phosphoramidic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / NaN₃ / dimethylsulfoxide / 60 °C

2: 100 percent / P(OMe)3 / tetrahydrofuran; H₂O / 45 °C

With sodium azide; phosphorous acid trimethyl ester; In tetrahydrofuran; water; dimethyl sulfoxide;
DOI:10.1016/S0040-4020(01)85427-2