2,9,15,18,21,24-hexaoxatetracyclo[24.2.2.2^4,7.2^10,13]tetratriaconta-1⁽²⁸⁾,4,6,10,12,26,29,31,33-nonaene

Base Information

• Chemical Name: 2,9,15,18,21,24-hexaoxatetracyclo[24.2.2.2^4,7.2^10,13]tetratriaconta-1⁽²⁸⁾,4,6,10,12,26,29,31,33-nonaene
• CAS No.: 879218-32-3
• Molecular Formula: C₂₈H₃₂O₆
• Molecular Weight: 464.558

Synonyms:2,9,15,18,21,24-hexaoxatetracyclo[24.2.2.2^4,7.2^10,13]tetratriaconta-1⁽²⁸⁾,4,6,10,12,26,29,31,33-nonaene

Chemical Property of 2,9,15,18,21,24-hexaoxatetracyclo[24.2.2.2^4,7.2^10,13]tetratriaconta-1⁽²⁸⁾,4,6,10,12,26,29,31,33-nonaene

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Technology Process of 2,9,15,18,21,24-hexaoxatetracyclo[24.2.2.2^4,7.2^10,13]tetratriaconta-1⁽²⁸⁾,4,6,10,12,26,29,31,33-nonaene

There total 1 articles about 2,9,15,18,21,24-hexaoxatetracyclo[24.2.2.2^4,7.2^10,13]tetratriaconta-1⁽²⁸⁾,4,6,10,12,26,29,31,33-nonaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

triethylene glycol di-(p-toluenesulfonate) (19249-03-7) + [1,4-phenylene-bis(methyleneoxy-4,1-phenylene)]dimethanol (170651-96-4) → 2,9,15,18,21,24-hexaoxatetracyclo[24.2.2.24,7.210,13]tetratriaconta-1(28),4,6,10,12,26,29,31,33-nonaene (879218-32-3)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 168h;

DOI:10.1021/jo052411+

Reference yield: 25.0%

2,9,15,18,21,24-hexaoxatetracyclo[24.2.2.24,7.210,13]tetratriaconta-1(28),4,6,10,12,26,29,31,33-nonaene (879218-32-3) + C16H17N7*F6P(1-)*H(1+) + tri-n-hexyl phosphite (6095-42-7) → C40H71N3O6P2*C28H32O6*F6P(1-)*H(1+)

Guidance literature:

In dichloromethane; at 20 ℃; for 16h;

DOI:10.1021/jo052411+

Reference yield: 14.0%

2,9,15,18,21,24-hexaoxatetracyclo[24.2.2.24,7.210,13]tetratriaconta-1(28),4,6,10,12,26,29,31,33-nonaene (879218-32-3) + C16H17N7*F6P(1-)*H(1+) + tri-n-butyl phosphite (102-85-2) → C32H55N3O6P2*C28H32O6*F6P(1-)*H(1+)

Guidance literature:

In dichloromethane; at 20 ℃; for 16h;

DOI:10.1021/jo052411+

upstream raw materials:

triethylene glycol di-(p-toluenesulfonate)

[1,4-phenylene-bis(methyleneoxy-4,1-phenylene)]dimethanol

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