N₁,N₁-dimethyl-N₂-(6,7-dihydro-5H-cyclopenta[1,2-d]pyrimidin-4-yl)-4-chlorobenzamidine

Base Information

• Chemical Name: N₁,N₁-dimethyl-N₂-(6,7-dihydro-5H-cyclopenta[1,2-d]pyrimidin-4-yl)-4-chlorobenzamidine
• CAS No.: 457072-55-8
• Molecular Formula: C₁₆H₁₇ClN₄
• Molecular Weight: 300.791

Synonyms:N₁,N₁-dimethyl-N₂-(6,7-dihydro-5H-cyclopenta[1,2-d]pyrimidin-4-yl)-4-chlorobenzamidine

Chemical Property of N₁,N₁-dimethyl-N₂-(6,7-dihydro-5H-cyclopenta[1,2-d]pyrimidin-4-yl)-4-chlorobenzamidine

Chemical Property:

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Technology Process of N₁,N₁-dimethyl-N₂-(6,7-dihydro-5H-cyclopenta[1,2-d]pyrimidin-4-yl)-4-chlorobenzamidine

There total 1 articles about N₁,N₁-dimethyl-N₂-(6,7-dihydro-5H-cyclopenta[1,2-d]pyrimidin-4-yl)-4-chlorobenzamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.0%

4-amino-6,7-dihydro-5H-cyclopenta[1,2-d]pyrimidine (26979-06-6) + N,N-dimethyl-4-chlorobenzamide (14062-80-7) → N1,N1-dimethyl-N2-(6,7-dihydro-5H-cyclopenta[1,2-d]pyrimidin-4-yl)-4-chlorobenzamidine (457072-55-8)

Guidance literature:

With triethylamine; trichlorophosphate; In chloroform; for 50h; Reflux;

DOI:10.1002/jhet.564

Reference yield: 73.0%

N1,N1-dimethyl-N2-(6,7-dihydro-5H-cyclopenta[1,2-d]pyrimidin-4-yl)-4-chlorobenzamidine (457072-55-8) → N-{2-[3-(4-chlorophenyl)[1,2,4]oxadiazol-5-yl]cyclopenten-1-yl}formamide oxime (457072-22-9)

Guidance literature:

With hydroxylamine hydrochloride; In methanol; at 20 ℃; for 19h;

DOI:10.1002/jhet.564

upstream raw materials:

4-amino-6,7-dihydro-5H-cyclopenta[1,2-d]pyrimidine

N,N-dimethyl-4-chlorobenzamide

Downstream raw materials:

N-{2-[3-(4-chlorophenyl)[1,2,4]oxadiazol-5-yl]cyclopenten-1-yl}formamide oxime

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