potassium 4,5,5-triethyl-2,5-dihydro-2,3-dimethyl-2-phenyl-1H-1,2,5-azasilaboratole

Base Information

Chemical Name:potassium 4,5,5-triethyl-2,5-dihydro-2,3-dimethyl-2-phenyl-1H-1,2,5-azasilaboratole
CAS No.:125824-71-7
Molecular Formula:C₁₆H₂₇BNSi*K
Molecular Weight:311.392
Hs Code.:

Synonyms:potassium 4,5,5-triethyl-2,5-dihydro-2,3-dimethyl-2-phenyl-1H-1,2,5-azasilaboratole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of potassium 4,5,5-triethyl-2,5-dihydro-2,3-dimethyl-2-phenyl-1H-1,2,5-azasilaboratole

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Technology Process of potassium 4,5,5-triethyl-2,5-dihydro-2,3-dimethyl-2-phenyl-1H-1,2,5-azasilaboratole

There total 1 articles about potassium 4,5,5-triethyl-2,5-dihydro-2,3-dimethyl-2-phenyl-1H-1,2,5-azasilaboratole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 125212-48-8
(E)-3-diethylboryl-2-methyldiphenylsilyl-2-pentene

: potassium amide

: 125824-71-7
potassium 4,5,5-triethyl-2,5-dihydro-2,3-dimethyl-2-phenyl-1H-1,2,5-azasilaboratole

Guidance literature:: In toluene; react. of a soln. of KNH2 and the (E)-borylsilylalkene at -30°C for 2,5 h; removing of the volatiles, drying (-30°C, 0.001 Torr), addn. of pentane, filtration, washing of the residue with pentane, drying in vac.; elem. anal.;

Reference yield: 86.0%

: 125824-71-7
potassium 4,5,5-triethyl-2,5-dihydro-2,3-dimethyl-2-phenyl-1H-1,2,5-azasilaboratole

: 125824-78-4
4,5,5-triethyl-2,5-dihydro-2,3-dimethyl-2-phenyl-1H-1,2,5-azoniasilaboratole

Guidance literature:: With hydrogenchloride; In diethyl ether; byproducts: KCl; to the K-1,2,5-azasilaboratole in Et2O is dropped a soln. of HCl in Et2O, boiling for 4,5 h; filtration, concn. at 12 Torr, distn.; elem. anal.;